Method for improving aeolotropism magnetic resistance permalloy film performance

An anisotropic magnetic and permalloy technology, which is applied in the manufacture/processing of electromagnetic devices, metal material coating technology, ion implantation plating, etc., can solve problems such as unfavorable AMR device applications, and achieve low crystal anisotropy , high anisotropic magnetoresistance value, low coercive force effect

Inactive Publication Date: 2009-02-25
UNIV OF SCI & TECH BEIJING
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Problems solved by technology

However, the Δρ/ρ of the AMR film decreases sharply with the decrease of the film thickness. For example, th...
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Abstract

The invention relates to a method for improving the performance of the thin permalloy film of an anisotropic magneto resistor, and belongs to the field of the magnetic thin film. The invention is characterized in that (Ni81Fe19)64Cr36 with a certain thickness is adopted as a buffer layer for induce the strong (111) Ni81Fe19 diffraction peak, and at the same time, an Al2O3 nano oxide layer is deposited onto the surface of Ni81Fe19, so as to increase the AMR value of the Ni81Fe19 thin film through the specular scattering function of the nano oxide layer. The Ni81Fe19 thin film with accurate components can be produced by the magnetron sputtering method. The structure of the thin film is (Ni81Fe19)64Cr36(1-13nm)/Ni81Fe19(10-200nm)/Al2O3(1-3nm)/Ta (5-9nm), argon gas with the purity of 99.99 percent is introduced into a film coating chamber for 0.5-1 hours before sputtering, and the content of impurity in the film is controlled within 0.1 percent. While reducing the preparation difficulty for the thin film, the method can also guarantee that the thin film has good all round performances such as high anisotropic magneto resistance value and low coercive force, low crystal anisotropy, large intensity of magnetization and low magnetostriction when the thin film is very thin, so as to meet the requirements of performances of a magnetic sensor and the products.

Application Domain

Technology Topic

Scattering functionPermalloy +17

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  • Method for improving aeolotropism magnetic resistance permalloy film performance
  • Method for improving aeolotropism magnetic resistance permalloy film performance

Examples

  • Experimental program(1)

Example Embodiment

[0012] DETAILED DESCRIPTION: Preparation of anisotropic permalloy Ni in a magnetron sputtering apparatus 81 Fe 19 film. First, the glass substrate is ultrasonically cleaned with organic chemical solvents and deionized water, and then mounted on the sample base of the sputtering chamber. The substrate was cooled with circulating deionized water, a magnetic field of 250 Oe was applied parallel to the direction of the substrate, and the substrate was always rotated at a rate of 18 revolutions/min, and the sputtering deposition rate was 0.17 nm/min. Sputtering chamber background vacuum 4×10 -5 Pa, pass 99.99% purity argon into the coating chamber for 0.5 hours before sputtering, and maintain the pressure at 0.3 Pa. During sputtering, 99.99% pure high-purity argon gas pressure is 0.4Pa, followed by deposition of 6nm thickness Ta/50.0nm thickness Ni y Fe 100-y. Through the 50.0nmNi y Fe 100-y Chemical analysis found the corresponding Ni when the film composition meets 81Ni:19Fe and the film impurity content is less than 0.1% x Fe 100-x Alloy target. Use this selected permalloy target to deposit Ni 81 Fe 19 film. Buffer layer (Ni 81 Fe 19 ) 64 Cr 36 By Ni 81 Fe 19 The target and Cr target are prepared by co-sputtering method. From figure 1 (a)Ta(z)/Ni 81 Fe 19 (20nm)/Ta(9nm) in Ni 81 Fe 19 (20nm) The AMR value of the thin film varies with the thickness of Ta. It can be seen that with the increase of z, the AMR value first increases and then decreases. When z=5.4nm, the AMR value of the film is the largest, which is 2.23±0.08 %. figure 1 (b) is (Ni 81 Fe 19 ) 64 Cr 36 (z)/Ni 81 Fe 19 (20nm)/Ta(9nm) in Ni 81 Fe 19 (20nm) film AMR value varies with (Ni 81 Fe 19 ) 64 Cr 36 The thickness curve shows that with the increase of z, the AMR value first increases and then decreases. When z=5.5nm, the AMR value of the film is the largest, 2.53%. versus figure 1 (a) Compared to figure 1 (a) Ni with 5.4nm Ta as the buffer layer 81 Fe 19 (20nm) The AMR value of the film is increased by 13%. It can be seen that (Ni 81 Fe 19 ) 64Cr 36 The buffer layer can improve Ni more than the Ta buffer layer 81 Fe 19 (20nm) Thin film AMR value. figure 2 Ta(6nm)/Ni 81 Fe 19 (20nm)/Al 2 O 3 The AMR value in (z)/Ta(6nm) film varies with Al 2 O 3 The curve of thickness z change. It can be seen that with the increase of z, the AMR value first increases and then decreases. When z=1.5nm, the AMR value of the film is the largest, which is 2.20%. Than without Al inserted 2 O 3 Time Ni 81 Fe 19 (20nm) The AMR value of the thin film is increased by about 10%. It can be seen that the deposition of Al 2 O 3 Nano oxide layer can improve Ni 81 Fe 19 (20nm) Thin film AMR value. Combining the advantages of the two, we prepared the structure as (Ni 81 Fe 19 ) 64 Cr 36 /Ni 81 Fe 19 /Al 2 O 3 /Ta samples. In film (Ni 81 Fe 19 ) 64 Cr 36 (5.5nm)/Ni 81 Fe 19 (20nm)/Al 2 O 3 The AMR value in (1.5nm)/Ta(9nm) reaches 2.75%, which is comparable to the traditional structure of the film Ta(5nm)/Ni 81 Fe 19 Compared with (20nm)/Ta(9nm) (its AMR value is 2.2%), it is increased by 25%.
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