Method for forming convex point structure formed by etching composition for convex point lower metal layer
A technology of under-bump metal and composition, which is applied in the direction of surface etching composition, chemical instruments and methods, electrical components, etc., and can solve the problems of damaged probe tip, wear, and reduced productivity.
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Embodiment 1
[0080] A solution was prepared comprising about 79.49% by weight of hydrogen peroxide (H 2 o 2 ), about 3% by weight of aqueous lye including tetramethylammonium hydroxide (TMAH), about 0.5% by weight of ethylene glycol (EG), about 17% by weight of dipotassium ethylenediaminetetraacetic acid (EDTA- 2K) and about 0.01% by weight of nonionic surfactant NCW (trade name; manufactured by Wako Pure Chemical Industries, Ltd. of Japan). The solution was stirred for about 30 minutes to prepare the etching composition for the UBM layer. The aqueous lye comprising tetramethylammonium hydroxide comprises about 25% by weight tetramethylammonium hydroxide.
Embodiment 2
[0082] In addition to using about 72.49% by weight of hydrogen peroxide and about 10% by weight of ammonium hydroxide (NH 4 OH) except for the aqueous alkali solution, an etching composition was prepared in substantially the same manner as in Example 1. The aqueous lye comprising ammonium hydroxide comprises about 38% by weight ammonium hydroxide.
experiment example 1
[0097] Evaluation of the etching performance and cleaning performance of the etching compositions in Example 1, Example 2 and Comparative Examples 1 to 5.
[0098] Substrates were prepared for evaluating the etching performance of the etching compositions according to Example 1, Example 2, and Comparative Examples 1 to 5. A titanium (Ti) layer, a titanium tungsten (TiW) layer, an aluminum (Al) layer, a silicon oxynitride (SiON), and a polyimide layer are respectively formed on each substrate. The substrates were etched by immersing the substrates in the etching compositions according to Example 1, Example 2, and Comparative Examples 1 to 5 at a temperature of about 40° C. to about 70° C. for about 1 to about 5 minutes, respectively. Clean each substrate by immersing the substrate in distilled water for approximately 5 min. Then, each substrate was dried using argon or nitrogen. A microscope was used to observe the surface of the substrate on which the aluminum layer, the sil...
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