Combustion synthesis apparatus for fullerenes

A combustion synthesis, fullerene technology, applied in the C70 and fullerene derivatives and other carbon cluster devices to prepare C60 field, can solve the problems of safety hazards, complex diffusion devices, synthesis ability defects, etc., to achieve operational flexibility High performance, good safety and low cost

Inactive Publication Date: 2009-08-12
XIAMEN UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

It has been reported (S.M.Lee, S.S.Yoon, and S.H.Chung, Synergistic effect on soot formation in counterflow diffusion flames of ethylene / propane mixtures with benzene addition.[J] Combustion and Flame 2004, 136,493-500) dedicated to the synthesis of fullerenes The diffusion device is either too complicated, or the system is mainly made of glass (see the applicant's Chinese invention patent, the notification number is CN101012056A), there are hidden dangers in safety and defects in synthesis ability

Method used

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  • Combustion synthesis apparatus for fullerenes
  • Combustion synthesis apparatus for fullerenes
  • Combustion synthesis apparatus for fullerenes

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Embodiment Construction

[0027] The following embodiments will further illustrate the present invention in conjunction with the accompanying drawings.

[0028] see figure 1 , The present invention is equipped with a combustion furnace, a combustion nozzle, a sleeve condenser, a canister, a liquid filter, a heat exchanger, a vacuum pump, a vacuum regulation system, an ignition system, a gas supply and control system, a vacuum test and display device.

[0029]The combustion furnace is the main part of the embodiment of the present invention, and consists of a chassis 1, a furnace body 3 and a furnace cover 7 sealed by an O-ring from bottom to top. Chassis 1 is a stainless steel disc with a round hole in the middle, and the length of the circular passage is increased by welding a round pipe 2 with the same inner diameter as the round hole. There is a groove in the passage, which is fixed and sealed by a rubber gasket and passes through it. combustion nozzle. The height design of the furnace body 3 shou...

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Abstract

The invention relates to a fullerene combustion synthesis device which is safe, easy to control and low in cost, and has a certain yield. The device is provided with a combustion furnace, a burner nozzle, a telescope-feed condenser tube, a filtration tank, a liquid filter, a heat exchanger, a vacuum pump, a vacuum regulating system, an ignition system, a gas supply and control system and a vacuum degree testing and displaying device; wherein, the burner nozzle is fixed on a base plate of the combustion furnace; the telescope-feed condenser tube is connected with downstream of a furnace cover of the combustion furnace; the filtration tank is connected with the telescope-feed condenser tube by a vacuum quick release flange; the liquid filter is connected with a filter tube by a pipeline; the heat exchanger is connected with the liquid filter by the pipeline; the vacuum pump is connected with the heat exchanger by a vacuum ball valve; the vacuum regulating system is provided with an air vent valve and the vacuum ball valve, and the ignition system is connected with a furnace body; the vacuum degree testing and displaying device is communicated with the furnace body of the combustion furnace; and the gas supply and control system is connected with the burner nozzle by an air supply duct.

Description

technical field [0001] The invention relates to a fullerene combustion synthesis device, in particular to a method for preparing C 60 、C 70 and devices of fullerene derivatives and other carbon clusters. Background technique [0002] Since their discovery in 1985, fullerenes have attracted widespread attention from the scientific community. The synthesis method and potential application value of fullerene have been extensively studied, and the theoretical research has also become more and more in-depth, providing the necessary theoretical guidance for experimental research, making it quickly become a hot field in chemical research. Since the discovery of C60, the exploration of fullerene synthesis methods has never stopped. The synthesis methods of fullerene mainly include laser evaporation graphite method, high frequency resistance furnace heating evaporation graphite method, graphite arc discharge method, solar heating graphite method, naphthalene pyrolysis method, micr...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B31/02
Inventor 翁群红孙頔林水潮陈建华谢素原黄荣彬郑兰荪
Owner XIAMEN UNIV
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