Quick degumming method for low-alkali cotton stalk bark fibre in high temperature

A degumming method and cotton stalk rind technology are applied in the field of degumming, which can solve the problems of high alkali consumption, complicated process and long time, and achieve the effect of low alkali concentration, simple process and good quality.

Inactive Publication Date: 2009-08-19
ZHEJIANG SCI-TECH UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although they made a positive step in using cotton stalk bark as textile materials, the method they adopted had the disadvantages of taking too long and using too much alkali. For example, the processing time in patent ZL94113220. The processing time in 200510034201.4 and 200610036594.7 also takes about 3 to 4 days, which brings many unfavorable factors to the application of cotton stalk fiber in textiles
Although the processing time of patents 200710066829.1 and 200710066830.4 is relatively reduced, the methods they use still have disadvantages such as complicated procedures and high energy consumption.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] (1) Rinse the cotton stalk skin three times with tap water, and then dry it.

[0024] (2) The dried cotton stalk bark is subjected to high-temperature and low-alkali scouring at a temperature of 140° C. and a pressure of 0.6 MPa. The quality of the scouring formula is the percentage of dry weight of cotton stalk bark: 10% sodium hydroxide, 20% sodium sulfide, 2% anthraquinone, 2% sodium silicate, and 2% sodium tripolyphosphate. The bath ratio is 1:14, the heating rate is 2°C / min, the temperature rises to 140°C, and the holding time is 20 minutes. Take it out and wash it with hot water first and then with cold water.

[0025] (3) Bleaching the treated cotton stalk fiber. The concentration of hydrogen peroxide is 9g / L, add sodium hydroxide 1g / L, magnesium sulfate 1g / L, bath ratio is 1:14, pH is 9, bleaching treatment temperature is 75°C, and treatment time is 40 minutes. Then wash with tap water and tumble dry.

[0026] (4) Oiling and softening the bleached and dried c...

Embodiment 2

[0029] (1) Rinse the cotton stalk skin three times with tap water, and then dry it.

[0030] (2) The dried cotton stalk bark is subjected to high-temperature and low-alkali scouring at a temperature of 150° C. and a pressure of 0.7 MPa. The quality of the scouring formula is the percentage of the dry weight of cotton stalk bark: 11% sodium hydroxide, 20% sodium sulfide, 2% anthraquinone, 2% sodium silicate, and 2% sodium tripolyphosphate. The bath ratio is 1:15, the heating rate is 2.5°C / min, the temperature is raised to 150°C, and the holding time is 30 minutes. Take it out and wash it with hot water and then with cold water.

[0031] (3) Bleaching the treated cotton stalk fiber. The hydrogen peroxide concentration is 10g / L, add sodium hydroxide 1g / L, magnesium sulfate 1g / L, liquor ratio 1:15, pH 10, bleaching treatment temperature 80°C, treatment time 45 minutes. Then wash with tap water and tumble dry.

[0032] (4) Oiling and softening the bleached and dried cotton stalk...

Embodiment 3

[0035] (1) Rinse the cotton stalk skin three times with tap water, and then dry it.

[0036] (2) The dried cotton stalk bark is subjected to high-temperature and low-alkali scouring at a temperature of 160° C. and a pressure of 0.8 MPa. The quality of the scouring formula is the percentage of the dry weight of cotton stalk bark: 12% sodium hydroxide, 20% sodium sulfide, 2% anthraquinone, 2% sodium silicate, and 2% sodium tripolyphosphate. The bath ratio is 1:16, the heating rate is 3°C / min, the temperature rises to 160°C, and the holding time is 40 minutes. Take it out and wash it with hot water first and then with cold water.

[0037] (3) Bleaching the treated cotton stalk fiber. The hydrogen peroxide concentration is 11g / L, add sodium hydroxide 1g / L, magnesium sulfate 1g / L, liquor ratio 1:16, pH 11, bleaching treatment temperature 85°C, treatment time 50 minutes. Then wash with tap water and tumble dry.

[0038] (4) Oiling and softening the bleached and dried cotton stalk...

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PUM

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Abstract

The invention discloses a fast colloid-removing method for high-temperature low-alkali cotton stack bark fiber. The technique flow thereof comprises: washing the cotton stack bark, drying, high-temperature low-alkali colloid-removing, washing, bleaching, washing, dehydrating, softening by applying oil, deoiling, drying and subtle drying of the cotton stack bark fiber, namely adopting the technique of boiling-bleaching-softening. The high-temperature high-pressure low-alkali technology is directly adopted to deeply degrade the hemicellulose and lignine in the cotton stack bark, and in the end hydrogen peroxiden is used for bleaching and softening the cotton stack bark fiber to prepare white and soft cotton stack bark fiber with high quality. The colloid removal rate of the cotton stack bark fiber after processing can achieve around 90%, and the removal rate of the hemicellulose content is around 97%. Compared with the disclosed patent technique of cotton stack bark fiber, as the invention adopts the technique of boiling-bleaching-softening, the processing period is greatly shortened; an orthogonal experiment is performed to control the alkaline amount to be the minimum and the colloid removal effect is optimum, thus saving resources and reducing discharge.

Description

technical field [0001] The invention relates to a degumming method, in particular to a high-temperature and low-alkali cotton stalk fiber rapid degumming method. Background technique [0002] Cotton stalk bark is a kind of good bast fiber, which is the main by-product fiber brought by planting cotton, accounting for about 30-35% of the total cotton stalk. In 2005, my country's cotton output surpassed that of the United States and ranked first in the world. And one mu of cotton field produces 225-250 kg of cotton stalks, and the skin part accounts for 26%, so the cotton stalk skin resources are extremely rich. In 2006, my country's total cotton output was 6.73 million tons, the actual total demand was 11.57 million tons, and the import volume had reached 3.64 million tons. Therefore, making full use of cotton stalk resources is of great significance to alleviate the serious shortage of cotton fibers in my country. But in the past people often used cotton stalk bark fiber a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01C1/02D06L3/02D06L4/12D06L4/13
Inventor 冯新星张玉高谌文惠陈建勇朱海霖郭玉海张华鹏
Owner ZHEJIANG SCI-TECH UNIV
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