Quick degumming method for low-alkali cotton stalk bark fibre in high temperature
A degumming method and cotton stalk rind technology are applied in the field of degumming, which can solve the problems of high alkali consumption, complicated process and long time, and achieve the effect of low alkali concentration, simple process and good quality.
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Embodiment 1
[0023] (1) Rinse the cotton stalk skin three times with tap water, and then dry it.
[0024] (2) The dried cotton stalk bark is subjected to high-temperature and low-alkali scouring at a temperature of 140° C. and a pressure of 0.6 MPa. The quality of the scouring formula is the percentage of dry weight of cotton stalk bark: 10% sodium hydroxide, 20% sodium sulfide, 2% anthraquinone, 2% sodium silicate, and 2% sodium tripolyphosphate. The bath ratio is 1:14, the heating rate is 2°C / min, the temperature rises to 140°C, and the holding time is 20 minutes. Take it out and wash it with hot water first and then with cold water.
[0025] (3) Bleaching the treated cotton stalk fiber. The concentration of hydrogen peroxide is 9g / L, add sodium hydroxide 1g / L, magnesium sulfate 1g / L, bath ratio is 1:14, pH is 9, bleaching treatment temperature is 75°C, and treatment time is 40 minutes. Then wash with tap water and tumble dry.
[0026] (4) Oiling and softening the bleached and dried c...
Embodiment 2
[0029] (1) Rinse the cotton stalk skin three times with tap water, and then dry it.
[0030] (2) The dried cotton stalk bark is subjected to high-temperature and low-alkali scouring at a temperature of 150° C. and a pressure of 0.7 MPa. The quality of the scouring formula is the percentage of the dry weight of cotton stalk bark: 11% sodium hydroxide, 20% sodium sulfide, 2% anthraquinone, 2% sodium silicate, and 2% sodium tripolyphosphate. The bath ratio is 1:15, the heating rate is 2.5°C / min, the temperature is raised to 150°C, and the holding time is 30 minutes. Take it out and wash it with hot water and then with cold water.
[0031] (3) Bleaching the treated cotton stalk fiber. The hydrogen peroxide concentration is 10g / L, add sodium hydroxide 1g / L, magnesium sulfate 1g / L, liquor ratio 1:15, pH 10, bleaching treatment temperature 80°C, treatment time 45 minutes. Then wash with tap water and tumble dry.
[0032] (4) Oiling and softening the bleached and dried cotton stalk...
Embodiment 3
[0035] (1) Rinse the cotton stalk skin three times with tap water, and then dry it.
[0036] (2) The dried cotton stalk bark is subjected to high-temperature and low-alkali scouring at a temperature of 160° C. and a pressure of 0.8 MPa. The quality of the scouring formula is the percentage of the dry weight of cotton stalk bark: 12% sodium hydroxide, 20% sodium sulfide, 2% anthraquinone, 2% sodium silicate, and 2% sodium tripolyphosphate. The bath ratio is 1:16, the heating rate is 3°C / min, the temperature rises to 160°C, and the holding time is 40 minutes. Take it out and wash it with hot water first and then with cold water.
[0037] (3) Bleaching the treated cotton stalk fiber. The hydrogen peroxide concentration is 11g / L, add sodium hydroxide 1g / L, magnesium sulfate 1g / L, liquor ratio 1:16, pH 11, bleaching treatment temperature 85°C, treatment time 50 minutes. Then wash with tap water and tumble dry.
[0038] (4) Oiling and softening the bleached and dried cotton stalk...
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