Molecular probe related to disease and method for producing the same
A molecular and disease technology, applied in the field of molecular probes and their preparation, can solve the problems of few aptamer molecules, few pure biomolecules, low screening efficiency, etc., and achieve a wide range of applications, high stability, and specific binding. strong effect
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Embodiment 1
[0041] Example 1. Preparation of molecular probes related to leukemia
[0042] 1. Screening of nucleic acid aptamers related to leukemia
[0043] (1) Synthesis of random nucleic acid library
[0044] According to the literature (Jayasena S D. Aptamers: an emerging class of molecules thatrival antibodies in diagnostics. Clin. Chem. 1999, 45: 1628-1650), the following random single-stranded DNA library was designed and synthesized: 5'-ATA CCA GCT TAT TCA ATT-52-nt-AGA TAGTAA GTG CAA TCT-3'.
[0045] (2) Screening of nucleic acid aptamers related to leukemia
[0046] Binding buffer: containing 4.5g / L glucose, 5mM MgCl 2 , 1mM CaCl 2 , 2.67mM KCl, 1.47mM potassium dihydrogen phosphate, 137.93mM sodium chloride, 8.06mM disodium hydrogen phosphate, 0.1mg / mL tRNA (R8759 Sigma, Ribonucleic acid, transfer from baker's yeast (S.cerevisiae)) and 1mg / mL bovine serum albumin (Fisher), pH 7.4.
[0047] CCRF-CEM cells (human T lymphocyte acute lymphoblastic leukemia) (CCL-119) and Ram...
Embodiment 2
[0084] Example 2. Molecular probes are used in the detection of leukemia cells
[0085] The three probes ppA, pB and pC obtained in Example 1 were used to detect leukemia cells respectively. Take 1μM molecular probe and incubate for 30 minutes with the isolated leukemia cells and the clinical bone marrow samples of insiders, centrifuge, wash the cells twice, and detect the cells with a flow cytometer.
[0086] The experiment was repeated 3 times and the results were consistent.
[0087] The detection results of the ppA molecular probe are as follows: image 3 Shown (wherein 1 represents the detection result of the leukemia cell CCRF-CEM, and the rest are the detection results of the normal cells (control cells) in the bone marrow). The pB and pC molecular probes have similar effects. It shows that the molecular probe of the present invention can effectively identify leukemia cells and specifically bind to it, and the molecular probe of the present invention can be used for ...
Embodiment 3
[0088] Example 3. Molecular probes are used in disease cell typing research
[0089] The molecular probe sequence related to lymphoma was prepared according to the method described in Example 1. The difference in the method was that lymphoma cells were taken as target disease cells, and 2 of them were labeled with fluorescein as molecules related to lymphoma probe.
[0090] Take 1 μM molecular probes related to lymphoma and the above-mentioned ppA, pB, pC molecular probes, incubate with leukemia cells and lymphoma cells for 30 minutes, centrifuge, wash cells twice, and use flow cytometry to detect different molecules Phenotypic characterization of probe binding to different cells.
[0091] The experiment was repeated 3 times and the results were consistent. The results show that the binding profiles of lymphoma cells and different molecular probes are similar, and the binding profiles of leukemia cells and different molecular probes are similar; it shows that the probes obta...
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