Polyurethane sealant and preparation method thereof
A polyurethane sealant, prepolymer technology, applied in the direction of polyurea/polyurethane adhesives, chemical instruments and methods, adhesives, etc., can solve the problem of low elongation, low body strength, affecting the application effect of one-component polyurethane sealants or ergonomics
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[0029] In order to further illustrate the technical means and effects of the present invention to achieve the intended purpose of the invention, the specific implementation of the polyurethane sealant proposed according to the present invention will be described in detail below in conjunction with the preferred embodiments.
[0030] Synthesis of prepolymers
[0031] The prepolymer is 30-60% by weight of polyoxypropylene diol (molecular weight 1500-4000), 20-55% of polyoxypropylene trihydric alcohol (molecular weight 4800-6500), 0.5-5 % of hexanediol, 10-30% of 4,4'-diphenylmethane diisocyanate and 0.1-0.5% of dibutyltin dilaurate (as a catalyst), under the protection of nitrogen in the reactor, at 90 ℃ -100 It can be obtained by reacting at ℃ for 2-5 hours. The prepolymer is a difunctional terminal isocyanate with a molecular weight of at least 1500 or more, a trifunctional terminal isocyanate with a molecular weight of at least 4800 or a mixture thereof, or an intermediate p...
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