Low-energy UV-curable circuit ink and preparation method thereof
A light-curing, low-energy technology, applied in inks, household utensils, applications, etc., can solve the problems of limiting the popularization and application of UV light curing, slow curing speed, low production efficiency, etc., to improve the curing speed, increase the curing speed, The effect of improving productivity
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Embodiment 1
[0035] Epoxy acrylate resin formula (mass percentage): novolak epoxy resin 30%, acid anhydride 40%, acrylic acid 24%, catalyst 3% and polymerization inhibitor 3%.
[0036] Photocurable line ink formula: 22 parts of epoxy acrylate resin, 3 parts of 2-methyl-1-[4-(methylthio)phenyl]-2-(4-morpholino)-1-acetone, 1 part of 2,4,6-trimethylbenzoyl-diphenylphosphine oxide, 32 parts of talc powder, 3 parts of silicon dioxide, 0.5 parts of titanium blue powder, 12 parts of hydroxyethyl methacrylate, trihydroxy 7 parts of methylpropane triacrylate, 2 parts of phosphate ester, 8 parts of barium sulfate, 0.15 part of polyether silicone oil and 0.2 part of BYK-104S.
[0037] Preparation method of photocurable circuit ink: (1) Preparation of epoxy acrylate resin
[0038](a) take by weighing each component that prepares epoxy acrylate resin by formula quantity, for subsequent use;
[0039] (b) under the environment of 60° C. to 90° C., add an acid anhydride accounting for 25% of the total m...
Embodiment 2
[0045] Epoxy acrylate resin formula (mass percentage): novolak epoxy resin 65%, acid anhydride 10%, acrylic acid 24.64%, catalyst 0.3% and polymerization inhibitor 0.06%.
[0046] Photocurable line ink formula: 28 parts of epoxy acrylate resin, 8 parts of 2-methyl-1-[4-(methylthio)phenyl]-2-(4-morpholinyl)-1-acetone, 3 parts of 2,4,6-trimethylbenzoyl-diphenylphosphine oxide, 38 parts of talc powder, 4 parts of silicon dioxide, 1.5 parts of titanium blue powder, 18 parts of hydroxyethyl methacrylate, trihydroxy 12 parts of methylpropane triacrylate, 6 parts of phosphate ester, 12 parts of barium sulfate, 0.4 part of polyether silicone oil and 0.5 part of S5200.
[0047] Preparation method of photocurable circuit ink: (1) Preparation of epoxy acrylate resin
[0048] (a) take by weighing each component that prepares epoxy acrylate resin by formula quantity, for subsequent use;
[0049] (b) under the environment of 60° C. to 90° C., add an acid anhydride accounting for 5% of the...
Embodiment 3
[0055] Epoxy acrylate resin formula (mass percentage): novolak epoxy resin 38%, acid anhydride 15%, acrylic acid 45%, catalyst 1% and polymerization inhibitor 1%.
[0056] Photocurable line ink formula: 25 parts of epoxy acrylate resin, 5 parts of 2-methyl-1-[4-(methylthio)phenyl]-2-(4-morpholino)-1-acetone, 2,4,6-trimethylbenzoyl-diphenylphosphine oxide 2 parts, talc powder 35 parts, silicon dioxide 3 parts, titanium blue powder 1 part, hydroxyethyl methacrylate 15 parts, trihydroxy 10 parts of methyl propane triacrylate, 4 parts of phosphate ester, 10 parts of barium sulfate, 0.2 part of polyether silicone oil and 0.35 part of BYK-104S.
[0057] Preparation method of photocurable line ink:
[0058] (1) Preparation of epoxy acrylate resin
[0059] (a) take by weighing each component that prepares epoxy acrylate resin by formula quantity, for subsequent use;
[0060] (b) Add acid anhydride accounting for 10% of the total mass of the reaction system to the novolac epoxy resi...
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