Method for preparing antifouling material with surface of spherically raised microstructure
A microstructure, spherical technology, applied in antifouling/underwater coatings, paints containing biocides, coatings, etc. Algae attachment performance, surface energy reduction, low cost effects
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Embodiment 1
[0012] Embodiment 1: Preparation of hydrogen-containing silicone oil and allyl acrylate polymer
[0013] Add 8.97g of allyl acrylate, 13.97g of toluene (solvent), and 8 μl of chloroplatinic acid catalyst into a 250ml four-necked flask, reflux, stir, blow nitrogen, heat up to 60°C, and dropwise add hydrogen-containing silicone oil (hydrogen-containing weight 1.60%) 5.0 g, after the dropwise addition, the reaction was kept for 1 h.
Embodiment 2
[0014] Embodiment 2: Preparation of hydrogen-containing silicone oil and allyl acrylate polymer
[0015] Add 2.24g of allyl acrylate, 22.24g of toluene, and 2μl of chloroplatinic acid catalyst into a 250ml four-neck flask, reflux, stir, blow nitrogen, heat up to 80°C, and dropwise add hydrogen-containing silicone oil (0.1% by weight of hydrogen) 20.0g, the dropwise addition was completed and the reaction was kept for 2 hours.
Embodiment 3
[0016] Embodiment 3: Preparation of hydrogen-containing silicone oil and allyl methacrylate polymer
[0017] Add 6.3g of allyl methacrylate, 16.3g of toluene (solvent), and 5 μl of chloroplatinic acid catalyst into a 500ml four-necked flask, reflux, stir, blow nitrogen, heat up to 65°C, and dropwise add hydrogen-containing silicone oil (containing Hydrogen weight (0.5%) 10.0g, the dropwise addition is completed and the reaction is kept for 1.5h.
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