Production method and device of regenerated fibroin fiber
A technology for regenerating silk and protein fibers, applied in the direction of cellulose/protein conjugated rayon, wet spinning, etc., can solve the problem of poor performance, inability to carry out large-scale industrial mass production, and relatively high requirements for process steps and equipment. Advanced problems, to achieve the effect of excellent performance
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[0018] combine figure 1 Shown, the production method of regenerated silk protein fiber of the present invention, comprises the following steps:
[0019] 1. Raw material selection
[0020] Select non-spinnable protein materials such as silk waste, silk waste, waste spinning, and silk spinning waste.
[0021] 2. Preparation of regenerated silk protein powder
[0022] Wash the silk waste, silk waste, waste spinning, silk spinning waste, etc. with water, then dry and weigh at room temperature, and then put the above silk material into lye (NaOH) with a concentration of 3-5% (weight percentage) In the process, according to the ratio of silk material: lye (weight ratio) of 1:50, hydrolyze at 60-70°C for 3-5 hours, filter after hydrolysis, remove lye and impurities, and obtain the regenerated silk protein stock solution, which is subjected to 100°C Under drying, the regenerated silk protein powder is obtained.
[0023] 2.1. Effect of hydrolysis temperature on hydrolysis of regene...
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