Preparation method of solid corrosion-inhibition scale-inhibition bar used for oil field
A solid technology for corrosion and scale inhibition, which is applied in the field of oil and gas wells and wellbore, can solve the problems of increasing the cost of corrosion and scale inhibition, increasing costs, affecting production, etc., and achieving low cost of corrosion and scale inhibition, less waste of chemicals, and long protection period. Effect
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Embodiment 1
[0043] The method discloses a method for preparing a solid corrosion and scale inhibition rod for oil fields, and the steps are as follows:
[0044] 1), 30% to 40% of 2-phosphonic acid butane-1,2,4-tricarboxylic acid, 10% to 15% of polyethylene glycol, 10% to 15% of sodium hexametaphosphate, 15% ~25% of Span-60 and 20%~30% of stearic acid are evenly mixed; the above percentages are the mass percentages of each component in the sum of all components;
[0045] 2) Put all the above-mentioned uniformly mixed components into a rod-shaped mold, and press it into a rod shape with a press to form a finished product, wherein the pressure applied by the press is 15 tons.
[0046] In step 1), the polyethylene glycol specifically refers to the industrial-grade polyethylene glycol PEG series commonly used in the field of petroleum drilling, especially the solid waxy polyglycols with high relative molecular weight and often used to increase viscosity and solidification. Ethylene glycol, su...
Embodiment 2
[0049] The method discloses a method for preparing a solid corrosion and scale inhibition rod for oil fields, and the steps are as follows:
[0050] 1) Select components and mix evenly, wherein, the selected components include:
[0051] 2-phosphonobutane-1,2,4-tricarboxylic acid PBTCA: 33%
[0052] Polyethylene glycol: 12%
[0053] Sodium hexametaphosphate: 12%
[0054] Span-60: 15%
[0055] Stearic acid: 28%
[0056] 2) Put all the above-mentioned uniformly mixed components into a rod-shaped mold, and press it into a rod shape with a press to form a finished product, wherein the pressure exerted by the press is 18 tons.
[0057] The finished solid corrosion and scale inhibition rod prepared in this example is determined by experiments: the corrosion inhibition rate is 93%, and the scale inhibition rate is 79%. When the water temperature is 35℃~55℃, the dissolution rate of the solid corrosion and scale inhibition rod is 0.068g / cm 2 m 3 .
Embodiment 3
[0059] The method discloses a method for preparing a solid corrosion and scale inhibition rod for oil fields, and the steps are as follows:
[0060] 1) Select components and mix evenly, wherein, the selected components include:
[0061] 2-phosphonobutane-1,2,4-tricarboxylic acid PBTCA: 38%
[0062] Polyethylene glycol: 10%
[0063] Sodium hexametaphosphate: 10%
[0064] Span-60: 17%
[0065] Stearic acid: 25%
[0066] 2) Put all the above-mentioned homogeneously mixed components into a rod-shaped mold, and press it into a rod shape with a press to form a finished product, wherein the pressure exerted by the press is 20 tons.
[0067] The solid corrosion and scale inhibition rods prepared in this example are determined by experiments: the corrosion inhibition rate is 97%, and the scale inhibition rate is 80%. When the water temperature is 35℃~55℃, the dissolution rate of solid corrosion and scale inhibition rod is 0.070g / cm 2 m 3 .
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