Process for producing superfine high-purity quartz glass pipe for high-temperature sensor
A quartz glass tube and high-temperature sensor technology, which is applied in glass forming, glass manufacturing equipment, radiation pyrometry, etc., can solve problems such as poor corrosion resistance, slow heat transfer speed, and poor heat uniformity, and achieve uniform heat Good performance, fast heat transfer and high strength
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Embodiment 1
[0018] Example 1. A production process of ultra-fine high-purity quartz glass tubes for high-temperature sensors, the steps of which are as follows:
[0019] (1) The selected particle size is 20-30mm, SiO 2 Quartz blocks with a content of more than 99% are used as raw materials; the raw materials are put into hydrochloric acid with a concentration of 10% by mass and soaked for 40 hours, and then the hydrochloric acid is eluted with pure water until the conductivity of the eluted water is less than 60 us / cm; Quartz material;
[0020] (2) Put the pickling quartz material into the roasting furnace, and roast it at 850°C for 5 hours. After the roasting, immediately quench it with pure water, then mechanically pulverize it, and sieve it to obtain 40-140 mesh quartz powder; then use The high magnetic machine performs iron removal treatment on the quartz powder;
[0021] (3) drop the quartz powder after iron removal into the mixed acid that is 10% hydrochloric acid, 10% nitric aci...
Embodiment 2
[0025] Example 2. A production process of ultra-fine high-purity quartz glass tubes for high-temperature sensors, the steps of which are as follows:
[0026] (1) The selected particle size is 20-30mm, SiO 2 Quartz blocks with a content of more than 99% are used as raw materials; the raw materials are put into hydrochloric acid with a mass percentage concentration of 30% and soaked for 20 hours, and then the hydrochloric acid is eluted with pure water until the conductivity of the eluted water is less than 60us / cm; Quartz material;
[0027] (2) Put the acid-washed quartz material into the roasting furnace, and roast it at 900° C. for 3 hours. After the roasting, immediately quench it with pure water, then mechanically pulverize it, and sieve it to obtain 40-140 mesh quartz powder; The magnetic machine removes iron from the quartz powder;
[0028] (3) drop the quartz powder after iron removal into the mixed acid that is 30% hydrochloric acid, 30% nitric acid and 15% hydrofluo...
Embodiment 3
[0032] Example 3. A production process of ultra-fine high-purity quartz glass tubes for high-temperature sensors, the steps of which are as follows:
[0033] (1) The selected particle size is 20-30mm, SiO 2 Quartz blocks with a content of more than 99% are used as raw materials; the raw materials are put into hydrochloric acid with a mass percentage concentration of 20% and soaked for 24 hours, and then the hydrochloric acid is eluted with pure water until the conductivity of the eluted water is less than 60us / cm; Quartz material;
[0034] (2) Put the pickling quartz material into the roasting furnace, and roast it at 880°C for 4 hours. After the roasting, immediately quench it with pure water, then mechanically pulverize it, and sieve it to get 40-140 mesh quartz powder; The magnetic machine removes iron from the quartz powder;
[0035] (3) drop the quartz powder after iron removal into the mixed acid that is 20% hydrochloric acid, 20% nitric acid and 10% hydrofluoric acid...
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