Method for preparing thin polymer film with polarization property on surface of glass
A polymer film and glass surface technology, applied in the field of polymer film preparation, can solve the problems of high production temperature, complex process, difficult to control the polarization effect, etc., achieve efficient synthesis and reduce complexity
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Embodiment 1
[0023] A method for preparing a polymer film with polarizing properties on a glass surface, comprising the steps of:
[0024] 1) Put 20mL of ethylene glycol into a beaker, put the beaker into an oil bath with a magnetic stirrer and raise the temperature to 155°C, then add 20 drops (about 1mL) of 0.005M to the above-mentioned heated ethylene glycol solution HAuCl 4 aqueous solution, the solution color changed from yellow to pink, which indicated the formation of gold nanoparticles. After constant temperature stirring for about 5 minutes, according to the mass of 0.2g AgNO 3 (First add 0.2g AgNO 3 Dispersed in 10mL of ethylene glycol solution) into the above oil bath, when the silver nitrate is added, the prepared PVP [dissolve 0.3g of PVP (polyvinylpyrrolidone) in 20mL of ethylene glycol] within 15min gradually Add dropwise to the above oil bath. The product was taken out after 60 minutes of reaction, and continuous stirring and constant temperature at 155° C. were required...
Embodiment 2
[0029] A method for preparing a polymer film with polarizing properties on a glass surface, comprising the steps of:
[0030]1) Put 20mL of ethylene glycol into a beaker, put the beaker into an oil bath with a magnetic stirrer and raise the temperature to 155°C, then add 20 drops (about 1mL) of 0.005M to the above-mentioned heated ethylene glycol solution HAuCl 4 aqueous solution, the solution color changed from yellow to pink, which indicated the formation of gold nanoparticles. After stirring at constant temperature for about 5 minutes, according to the mass of 0.4g AgNO 3 (First add 0.4g AgNO 3 Dispersed in 10mL ethylene glycol solution) into the above oil bath, when the silver nitrate is added, add the prepared PVP (dissolve 0.7g PVP in 20mL ethylene glycol first) to the above oil bath drop by drop within 15min in the pot. The product was taken out after 60 minutes of reaction, and continuous stirring and constant temperature at 155° C. were required during the entire ...
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