Giant dielectric-nonlinear low-voltage difunctional varistor ceramic material and preparation method thereof
A ceramic material and non-linear technology, which is applied in the field of giant dielectric varistors and non-linear varistor materials, can solve the problems of varistor characteristics that are not recorded, and achieve the effects of short cycle, simple process operation and low cost
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Embodiment 1
[0019] Preparation of Bi by sol-gel method using citric acid as complexing agent 0.5-x Na 0.5-x Ba 2x Cu 3 Ti 4 O 12 (x=0) Ceramic. First, weigh 0.08mol of citric acid into a 100mL beaker 1, add 35mL of deionized water, dissolve under ultrasonic dispersion to form a transparent solution; then weigh 0.04mol of butyl titanate into a 100mL beaker 2, then Transfer the citric acid solution in 1 beaker to the titanium solution in 2 beakers; dissolve the titanium solution under constant stirring, then ultrasonically disperse for 30 min, and then add 5 mL of ethylene glycol to form a transparent solution. The molar ratio of butyl titanate and citric acid aqueous solution is 1:2. In the second step, 0.05mol of citric acid was weighed into a 500mL beaker, 20mL of deionized water was added, and dissolved under ultrasonic dispersion to form a transparent solution; then 0.03mol of copper nitrate, 0.005mol of sodium nitrate, 0.005 mol of bismuth nitrate was added to the above soluti...
Embodiment 2
[0022] Preparation of Bi by sol-gel method using citric acid as complexing agent 0.5-x Na 0.5-x Ba 2x Cu 3 Ti 4 O 12 (x=0.025) Ceramic. First, weigh 0.08mol of citric acid into a 100mL beaker 1, add 35mL of deionized water, dissolve under ultrasonic dispersion to form a transparent solution; then weigh 0.04mol of butyl titanate into a 100mL beaker 2, then Transfer the citric acid solution in 1 beaker to the titanium solution in 2 beakers; dissolve the titanium solution under constant stirring, then ultrasonically disperse for 30 min, and then add 5 mL of ethylene glycol to form a transparent solution. The molar ratio of butyl titanate and citric acid aqueous solution is 1:2. In the second step, 0.05mol of citric acid was weighed into a 500mL beaker, 20mL of deionized water was added, and dissolved under ultrasonic dispersion to form a transparent solution; then 0.03mol of copper nitrate, 0.00475mol of sodium nitrate, 0.00475 mol of bismuth nitrate and 0.0005 mol of bar...
Embodiment 3
[0025] Preparation of Bi by sol-gel method using citric acid as complexing agent 0.5-x Na 0.5-x Ba 2x Cu 3 Ti 4 O 12 (x=0.005) Ceramic. First, weigh 0.08mol of citric acid into a 100mL beaker 1, add 35mL of deionized water, dissolve under ultrasonic dispersion to form a transparent solution; then weigh 0.04mol of butyl titanate into a 100mL beaker 2, then Transfer the citric acid solution in 1 beaker to the titanium solution in 2 beakers; dissolve the titanium solution under constant stirring, then ultrasonically disperse for 30 min, and then add 5 mL of ethylene glycol to form a transparent solution. The molar ratio of butyl titanate and citric acid aqueous solution is 1:2. In the second step, 0.05mol of citric acid was weighed into a 500mL beaker, 20mL of deionized water was added, and dissolved under ultrasonic dispersion to form a transparent solution; then 0.03mol of copper nitrate, 0.0045mol of sodium nitrate, 0.0045 mol of bismuth nitrate and 0.001 mol of barium...
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