Novel 2-(amino) ethyl methyl sulfone salt and preparation
A technology of ethyl methyl sulfone hydrochloride and ethyl methyl sulfone, which is applied in the field of preparing high-purity 2-ethyl methyl sulfone, and can solve the problems such as difficult purification of hydrochloride
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[0017] 2-(Amino)ethylmethylsulfone hydrogen sulfate
[0018] Add 30 liters of ethanol in the 50 liter kettle, add 0.58 kilograms of sodium hydroxide, stir to dissolve. Cool down to 20°C, add 2.3 kg of 2-(amino)ethylmethylsulfone hydrochloride in batches, and stir for 0.5 hours. Filter, wash the filter cake with ethanol, and combine the washing liquid and the filtrate. Cool to about 10°C, add 1.4 kg of p-toluenesulfonic acid in batches, and a white solid precipitates out. Stir for 2 hours, filter, and wash with ethanol to obtain 2.6 kg of 2-(amino)ethylmethylsulfone hydrogensulfate.
[0019] 2-(Amino)ethylmethylsulfone Sulfate
[0020] Add 30 liters of ethanol in the 50 liter kettle, add 0.58 kilograms of sodium hydroxide, stir to dissolve. Cool down to 20°C, add 2.3 kg of 2-(amino)ethylmethylsulfone hydrochloride in batches, and stir for 0.5 hours. Filter, wash the filter cake with ethanol, and combine the washing liquid and the filtrate. Cool to about 10°C, add 0.7 kg o...
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