Method for preparing reaction-type perfume material by using extraction residues

A residue and raw material technology, which is applied in the field of Maillard reaction to prepare tobacco flavors, can solve the problems of environmental protection, waste, and environmental pollution, and achieve the effects of environmental protection, low cost, and full aroma

Inactive Publication Date: 2011-04-06
HUBEI CHINA TOBACCO IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These extracted plant material residues are rich in cellulose or protein, etc., directly discarding them not only pollutes the environ

Method used

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  • Method for preparing reaction-type perfume material by using extraction residues
  • Method for preparing reaction-type perfume material by using extraction residues

Examples

Experimental program
Comparison scheme
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Example Embodiment

[0022] Example 1:

[0023] 1. Using nut shell extract residue as raw material, stir evenly after adding water, the solids account for 60%, add 25% of the total mass of phosphoric acid with a concentration of 60%, and stir in a water bath for hydrolysis at 80°C. The hydrolysis time is 4 hours. , Filter to remove a small amount of insoluble matter to obtain cellulose hydrolysate, mainly a mixture of glucose and xylose.

[0024] 2. Using soybean meal as the raw material, stir evenly after adding water, the solids account for 70%, add 20% of the total mass of 60% phosphoric acid, hydrolyze at 100 ℃, the hydrolysis time is 4 hours, filter to remove a small amount of insolubles , Get protein hydrolysate, mainly a mixture of amino acids.

[0025] 3. Mix the nutshell residue hydrolysate and soybean meal hydrolysate in a ratio of 1:1.2 and stir evenly, adjust the pH to 7.5, add 2% ascorbic acid, heat and reflux under normal pressure for 4 hours, after the reaction is completed, quickly cool ...

Example Embodiment

[0028] Example 2:

[0029] 1. Take the chaff residue as the raw material, stir evenly after adding water, the solid content is 55%, add 15% of the total mass of phosphoric acid with a concentration of 55%, and stir in a water bath for hydrolysis at 75°C. The hydrolysis time is 6 hours. A small amount of insoluble matter is filtered to obtain a cellulose hydrolysate, mainly reducing sugars such as glucose, xylose, and fructose.

[0030] 2. Using soybean meal as raw material, stir evenly after adding water, the solid content is 70%, and 20% of the total mass is added with a concentration of 55% phosphoric acid. Hydrolysis is carried out at 100°C. The hydrolysis time is 4 hours, and a small amount of insoluble matter is filtered out. , To obtain the soybean meal protein hydrolysate, mainly a mixture of amino acids.

[0031] 3. Mix the husk hydrolysate and soybean meal protein hydrolysate in a ratio of 1:1.2 and stir evenly, adjust the pH to 8, add 2% ascorbic acid, heat and reflux unde...

Example Embodiment

[0033] Example 3:

[0034] 1. Take the red jujube extraction residue as the raw material, add water and stir evenly, the solid content is 60%, add 25% of the total mass of phosphoric acid with a concentration of 65%, and stir in a water bath for hydrolysis at 80°C. The hydrolysis time is 4 hours. Filter to remove a small amount of insoluble matter to obtain a cellulose hydrolysate, mainly a mixture of glucose, xylose, and fructose.

[0035] 2. Using soybean meal as raw material, stir evenly after adding water, the solids account for 70%, add 20% of the total mass of phosphoric acid with a concentration of 65%, and hydrolyze at 100°C. The hydrolysis time is 4 hours. Filter to remove a small amount of insoluble To obtain soybean meal protein hydrolysate, mainly a mixture of amino acids.

[0036] 3. Mix the red jujube residue hydrolysate and soybean meal protein hydrolysate in a ratio of 1:1 and stir evenly, adjust the pH to 8, add 1% malonic acid, heat and reflux under normal pressure...

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Abstract

The invention discloses a method for preparing a reaction-type perfume material by using extraction residues, belonging to the technical field of preparation of the perfume material for tobacco. In the method, plant residues containing rich cellulose and residues containing rich protein are hydrolyzed respectively, the hydrolyzing degree of the cellulose and the protein is controlled by controlling the content of hydrolytic acid to obtain a series of reducing sugar and amino acid, and the two hydrolyzed systems are mixed and heated for Maillard reaction. The method of the invention can help obtain a series of excellent perfume materials with features and low cost for the tobacco, solve the problem of treating the residues of the obtained extract and avoid environmental pollution. The reaction-type perfume material can be used in cigarettes for enriching cigarette fragrance, enhancing cigarette smoke and improving taste.

Description

technical field [0001] The invention belongs to the technical field of preparation of flavorings for tobacco, and in particular relates to a method for obtaining a nitrogen source and a sugar source by hydrolyzing natural plants through extracting residues, and then preparing flavorings for tobacco through Maillard reaction. Background technique [0002] In the prior art, people pay more and more attention to the safety of cigarettes, and reducing the tar in cigarettes has become an inevitable trend. With the reduction of tar, the smell of cigarettes becomes lighter and the aroma is weakened, which is difficult to be accepted by consumers. . Thereby, in order to promote and improve the smoke concentration and fragrance of cigarettes, flavoring and adding materials have become an effective way. The Maillard reaction is a reaction between amino acids and reducing sugars. It has been confirmed that Maillard reactions occur in tobacco during conditioning, aging, processing and ...

Claims

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Application Information

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IPC IPC(8): C11B9/00A24B15/30
Inventor 肜霖黄龙张敦铁吴昭
Owner HUBEI CHINA TOBACCO IND
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