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Method for preparing reaction-type perfume material by using extraction residues

A residue and raw material technology, which is applied in the field of Maillard reaction to prepare tobacco flavors, can solve the problems of environmental protection, waste, and environmental pollution, and achieve the effects of environmental protection, low cost, and full aroma

Inactive Publication Date: 2011-04-06
HUBEI CHINA TOBACCO IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These extracted plant material residues are rich in cellulose or protein, etc., directly discarding them not only pollutes the environment, is not conducive to environmental protection, but also wastes the cellulose, or protein and other components in the plant residue

Method used

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  • Method for preparing reaction-type perfume material by using extraction residues
  • Method for preparing reaction-type perfume material by using extraction residues

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] 1. Use nut shell extraction residue as raw material, add water and stir evenly, the solid content accounts for 60%, add phosphoric acid with a concentration of 60% of 25% of the total mass, stir in a water bath at 80°C for hydrolysis, and the hydrolysis time is 4 hours , and filter out a small amount of insoluble matter to obtain a cellulose hydrolyzate, which is mainly a mixture of glucose and xylose.

[0024] 2. Use soybean meal as raw material, add water and stir evenly, the solid matter accounts for 70%, add phosphoric acid with a concentration of 60% of 20% of the total mass, carry out hydrolysis under the condition of 100°C, the hydrolysis time is 4 hours, filter out a small amount of insoluble matter , to obtain a protein hydrolyzate, mainly a mixture of amino acids.

[0025] 3. Mix and stir the nut shell residue hydrolyzate and soybean meal hydrolyzate at a ratio of 1:1.2, adjust the pH value to 7.5, add 2% ascorbic acid, and heat and reflux for 4 hours under no...

Embodiment 2

[0029] 1. Take chaff residue as raw material, stir evenly after adding water, the solid matter accounts for 55%, add phosphoric acid with a concentration of 55% of 15% of the total mass, stir in a water bath at 75°C for hydrolysis, and the hydrolysis time is 6 hours. A small amount of insoluble matter is filtered to obtain a cellulose hydrolyzate, mainly reducing sugars such as glucose, xylose, and fructose.

[0030] 2. Use soybean meal as raw material, add water and stir evenly, the solid matter accounts for 70%, add phosphoric acid with a concentration of 55% of 20% of the total mass, carry out hydrolysis under the condition of 100°C, the hydrolysis time is 4 hours, filter out a small amount of insoluble matter , to obtain soybean meal protein hydrolyzate, which is mainly a mixture of amino acids.

[0031] 3. Mix and stir the chaff hydrolyzate and soybean meal protein hydrolyzate in a ratio of 1:1.2, adjust the pH value to 8, add 2% ascorbic acid, and heat and reflux for 4 h...

Embodiment 3

[0034] 1. Use red jujube extraction residue as raw material, add water and stir evenly, the solid matter accounts for 60%, add 25% of the total mass of phosphoric acid with a concentration of 65%, stir in a water bath at 80°C for hydrolysis, and the hydrolysis time is 4 hours, A small amount of insoluble matter is removed by filtration to obtain a cellulose hydrolyzate, which is mainly a mixture of glucose, xylose and fructose.

[0035] 2. Use soybean meal as raw material, add water and stir evenly, the solids account for 70%, add 20% of the total mass of phosphoric acid with a concentration of 65%, hydrolyze at 100°C, hydrolysis time is 4 hours, filter to remove a small amount of insoluble The product is obtained to obtain soybean meal protein hydrolyzate, which is mainly a mixture of amino acids.

[0036] 3. Mix and stir the jujube residue hydrolyzate and soybean meal protein hydrolyzate in a ratio of 1:1, adjust the pH value to 8, add 1% malonic acid, heat and reflux at nor...

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Abstract

The invention discloses a method for preparing a reaction-type perfume material by using extraction residues, belonging to the technical field of preparation of the perfume material for tobacco. In the method, plant residues containing rich cellulose and residues containing rich protein are hydrolyzed respectively, the hydrolyzing degree of the cellulose and the protein is controlled by controlling the content of hydrolytic acid to obtain a series of reducing sugar and amino acid, and the two hydrolyzed systems are mixed and heated for Maillard reaction. The method of the invention can help obtain a series of excellent perfume materials with features and low cost for the tobacco, solve the problem of treating the residues of the obtained extract and avoid environmental pollution. The reaction-type perfume material can be used in cigarettes for enriching cigarette fragrance, enhancing cigarette smoke and improving taste.

Description

technical field [0001] The invention belongs to the technical field of preparation of flavorings for tobacco, and in particular relates to a method for obtaining a nitrogen source and a sugar source by hydrolyzing natural plants through extracting residues, and then preparing flavorings for tobacco through Maillard reaction. Background technique [0002] In the prior art, people pay more and more attention to the safety of cigarettes, and reducing the tar in cigarettes has become an inevitable trend. With the reduction of tar, the smell of cigarettes becomes lighter and the aroma is weakened, which is difficult to be accepted by consumers. . Thereby, in order to promote and improve the smoke concentration and fragrance of cigarettes, flavoring and adding materials have become an effective way. The Maillard reaction is a reaction between amino acids and reducing sugars. It has been confirmed that Maillard reactions occur in tobacco during conditioning, aging, processing and ...

Claims

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Application Information

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IPC IPC(8): C11B9/00A24B15/30
Inventor 肜霖黄龙张敦铁吴昭
Owner HUBEI CHINA TOBACCO IND
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