Unlock instant, AI-driven research and patent intelligence for your innovation.

Method for obtaining clean gas via destructive distillation of coal

A clean gas and coal dry distillation technology, which is applied in special forms of dry distillation, combustible gas purification, combustible gas purification/transformation, etc., can solve problems such as polluting the environment and increasing water treatment costs, and achieve the effect of reducing costs

Inactive Publication Date: 2013-03-13
CHINA NAT OFFSHORE OIL CORP +1
View PDF2 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It can be seen that the treatment of oily wastewater leads to an increase in water treatment costs and is also the main source of environmental pollution in the coal dry distillation industry

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for obtaining clean gas via destructive distillation of coal

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] This embodiment is used to illustrate the method for obtaining clean coal gas by dry distillation of coal provided by the present invention.

[0033] use figure 1 In the process shown, long-flame coal with a size of 25-80 mm (see Table 1 for relevant physical properties) is dry-distilled in a vertical furnace. The temperature at the bottom of the vertical furnace is 900 ° C. 100°C, the bottom pressure is 0.14MPa, and the top pressure is 0.11MPa. The raw coal gas with a pressure of 0.11MPa and a temperature of 100°C, that is, a mixed gas containing tar, is obtained. The composition of the raw coal gas except water is shown in Table 3. Water The content is 30% by weight of the total raw gas.

[0034] Then the raw coal gas is contacted with coal tar at a flow rate of 100 kg / h at a temperature of 180°C, a distillation range of 180-500°C, and a flow rate of 200 kg / h. After contacting for 100 seconds, the liquid phase product is the first liquid product Discharged from the ...

Embodiment 2

[0036] This embodiment is used to illustrate the method for obtaining clean coal gas by dry distillation of coal provided by the present invention.

[0037] use figure 1 In the process shown, long-flame coal with a size of 25-80mm (see Table 1 for relevant physical properties) is dry-distilled in a vertical furnace. The temperature at the bottom of the vertical furnace is 700°C. 160°C, the pressure at the bottom is 0.12MPa, and the pressure at the top is 0.106MPa, and the raw coal gas with a pressure of 0.108MPa and a temperature of 160°C is obtained. The composition of the raw coal gas except water is shown in Table 3. 0.05 times the weight of the total amount of the mixture.

[0038] Then this raw coal gas is contacted with coal tar whose temperature is 90° C., distillation range is 180-500° C., and flow rate is 100 kg / h with a flow rate of 100 kg / h. After contacting for 60 seconds, the liquid phase product is discharged from the bottom of the tower. The gas phase product ...

Embodiment 3

[0040] This embodiment is used to illustrate the method for obtaining clean coal gas by dry distillation of coal provided by the present invention.

[0041] use figure 1 In the process shown, long-flame coal with a size of 25-80mm (see Table 1 for relevant physical properties) is dry-distilled in a vertical furnace. The temperature at the bottom of the vertical furnace is 850°C. 180°C, the pressure at the bottom is 0.13MPa, and the pressure at the top is 0.102MPa, and the raw coal gas with a pressure of 0.102MPa and a temperature of 180°C is obtained. The composition of the raw coal gas except water is shown in Table 3, and the water content is the total amount of clean gas 0.1 times the weight.

[0042] Then this crude coal gas is contacted with coal tar that temperature is 100 DEG C, distillation range is 180-500 DEG C, flow rate is 100 kg / hour with the flow rate of 100 kg / hour, after contacting for 20 seconds, the liquid phase product is discharged from the bottom of the t...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
boiling pointaaaaaaaaaa
Login to View More

Abstract

The invention discloses a method for obtaining clean gas via the destructive distillation of coal, comprising the steps of: (1) carrying out destructive distillation on the coal in destructive distillation condition to obtain crude gas, wherein the crude gas contains carbon monoxide, hydrogen, methane, carbon dioxide, tar and water, and the boiling point of the tar is higher than that of the water; (2) contacting the crude gas with an organic solvent to obtain a first gas product and a first liquid product, wherein the contact condition of the crude gas and the organic solvent is that the temperature of the organic solvent is 70-150DEG C and the time is 10-120sec; and (3) cooling the first gas product to obtain the clean gas and a second liquid product, and separating out the second liquid product. By adopting the method in the invention, the coal tar with water content less than 1% by weight can be directly obtained, and the oil content in the separated water is less than 200mg / L.

Description

technical field [0001] The invention relates to a method for obtaining clean coal gas by dry distillation of coal. Background technique [0002] Coal dry distillation is the process of heating coal in the absence of air to decompose it into gases such as gas, liquids such as tar and solids such as coke. Dry distillation is generally carried out in a vertical furnace, which generally includes a drying section, a dry distillation section and a cooling section from top to bottom. The raw coal first enters the drying section at the upper part of the furnace, and the raw coal is preheated by the hot airflow generated in the dry distillation section, and then moves down to the dry distillation section for dry distillation. The high-temperature semi-coke obtained from the dry distillation is immersed in water and extinguished and produces a large amount of water vapor. The rise of water vapor and the combination of high-temperature semi-coke produce a large amount of water gas. Th...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C10K1/16C10K1/18C10K1/00C10B53/04C10B53/08
Inventor 马跃龙梅永刚欧书能郑长波熊亮吴洪胜左柯庆
Owner CHINA NAT OFFSHORE OIL CORP