Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Surface microporous SiC ceramic material and preparation method thereof

A technology of ceramic materials and surface micropores, which is applied in the field of surface microporous SiC ceramic materials and its preparation, can solve the problems of increasing friction coefficient, shortening service life, and affecting product yield, so as to reduce dynamic friction coefficient and improve service life Effect

Active Publication Date: 2012-11-14
ZHEJIANG UNIV
View PDF1 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the hardness of silicon carbide ceramics has been improved, some silicon carbide ceramic mechanical parts (such as silicon carbide seals) still have the following problems during use: 1), some silicon carbide ceramic mechanical parts (such as silicon carbide seals) When hard-to-hard seals are rubbed, the working surfaces at both ends are easily bonded, which increases the friction coefficient and shortens the service life
2) The debris generated during friction cannot be removed in time, which will accelerate the wear of mechanical parts, thus affecting the service life of seals
The above method has the following disadvantages: the cross-linked pores formed by the decomposition of the cross-linking agent at high temperature have different sizes, irregular shapes, and uneven distribution, and the product is prone to cracking during the sintering process, which affects the yield of the product

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Embodiment 1, a kind of preparation method of surface microporous SiC ceramic material, carries out following steps successively:

[0027] 1), ingredients:

[0028] The main raw material is composed of 85 parts of silicon carbide powder and 15 parts of yttrium aluminum garnet, 10 parts of polycarbosilane as a binder and foaming agent, and 8 parts of carboxymethyl cellulose as a pore-forming agent.

[0029] 2), mix the above-mentioned silicon carbide powder, yttrium aluminum garnet and polycarbosilane evenly, and mix into a mixture;

[0030] 3), add carboxymethyl cellulose to deionized water, stir until completely dissolving, obtain the methyl cellulose aqueous solution that mass concentration is 7% (that is, the mass concentration of carboxymethyl cellulose in methyl cellulose aqueous solution is 7%);

[0031] 4), after ball milling and mixing the mixture with the carboxymethyl cellulose aqueous solution for 5 hours, a slurry was obtained;

[0032] 5) Dry the slurry ...

Embodiment 2

[0036] Embodiment 2, a method for preparing a surface microporous SiC ceramic material, the following steps are carried out in sequence:

[0037] 1), ingredients:

[0038] The main raw materials are composed of 90 parts of silicon carbide powder and 10 parts of yttrium aluminum garnet, 5 parts of polycarbosilane as a binder and foaming agent, and 2 parts of carboxymethyl cellulose as a pore-forming agent.

[0039] 2), mix the above-mentioned silicon carbide powder, yttrium aluminum garnet and polycarbosilane evenly, and mix into a mixture;

[0040] 3), adding carboxymethyl cellulose into deionized water, stirring until completely dissolved, to obtain an aqueous solution of methyl cellulose with a mass concentration of 3%;

[0041] 4), after ball milling and mixing the mixture with the carboxymethyl cellulose aqueous solution for 7 hours, a slurry was obtained;

[0042] 5) Dry the slurry at a temperature of 120° C. for 4 hours, then fully stir and mix again with a mixer; obta...

Embodiment 3

[0046] Embodiment 3, a method for preparing a surface microporous SiC ceramic material, the following steps are carried out in sequence:

[0047] 1), ingredients:

[0048] The main raw materials are 88 parts of silicon carbide powder and 12 parts of yttrium aluminum garnet, 7 parts of polycarbosilane as binder and foaming agent, and 5 parts of carboxymethyl cellulose as pore-forming agent.

[0049] 2), mix the above-mentioned silicon carbide powder, yttrium aluminum garnet and polycarbosilane evenly, and mix into a mixture;

[0050] 3), adding carboxymethyl cellulose into deionized water, stirring until completely dissolved, to obtain an aqueous solution of methyl cellulose with a mass concentration of 5%;

[0051] 4), after ball milling and mixing the mixture with carboxymethyl cellulose aqueous solution for 2 hours, a slurry was obtained;

[0052] 5), drying the slurry at a temperature of 100°C for 4 hours, and then fully stirring and mixing again with a mixer to obtain a ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
compressive strengthaaaaaaaaaa
flexural strengthaaaaaaaaaa
Knoop hardnessaaaaaaaaaa
Login to View More

Abstract

The invention discloses a surface microporous SiC ceramic material, which consists of main raw materials, polycarbosilane and carboxymethyl cellulose, wherein the main raw materials consist of the following components in percentage by weight: 85 to 90 percent of silicon carbide powder and 10 to 15 percent of yttrium aluminum garnet; the polycarbosilane is 5 to 10 percent of the total weight of the main raw materials; and the carboxymethyl cellulose is 2 to 8 percent of the total weight of the main raw materials. Meanwhile, the invention discloses a method for preparing the surface microporousSiC ceramic material, which comprises the following steps of: uniformly mixing the silicon carbide powder, the yttrium aluminum garnet and the polycarbosilane, and adding aqueous solution of the carboxymethyl cellulose and performing ball-milling mixing; drying the obtained size; and molding the obtained powder and performing vacuum sintering at high temperature so as to prepare the surface microporous SiC ceramic material. The surface microporous SiC ceramic material keeps high strength, high hardness, abrasion resistance, corrosion resistance and oxidation resistance, the self-lubricating property of the material is improved, and a cross section can be prevented from being bonded. Therefore, the service life of the material is prolonged.

Description

technical field [0001] The invention relates to a surface microporous SiC ceramic material and a preparation method thereof. Background technique [0002] Ceramic materials are widely used in national defense, machinery, chemical industry, metallurgy, electronics and other fields. In recent years, industrially developed countries such as Britain, the United States, Germany, France, and Japan have widely used structural ceramics in the structural parts of aviation, aerospace and high-precision machinery, and have achieved considerable economic and social benefits. Among many engineering ceramic materials, silicon carbide (SiC) ceramics have high strength, high hardness, good wear resistance, corrosion resistance, strong oxidation resistance, high thermal conductivity, good high temperature stability, small thermal expansion coefficient, and heat resistance. It has become the most promising high-temperature structural ceramics due to its excellent properties such as strong sh...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/565C04B38/02C04B35/622
Inventor 郭兴忠杨辉黄永银郑志荣高黎华
Owner ZHEJIANG UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products