Cleaning solution composition for cleaning substrate
A cleaning solution and composition technology, applied in the direction of photosensitive material processing, etc., can solve the problems of poor shape of photoresist film and insufficient cleaning power.
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Embodiment 1
[0036] Take 30 parts by weight of propylene glycol monomethyl ether (PGME) and 70 parts by weight of propylene glycol monomethyl ether acetate (PGMEA), respectively add molecular sieve 4A (granular), and stir for 6 hours for pretreatment. Among them, molecular sieve and PGME or PGMEA The weight ratio is 2 / 100. Then, they were filtered under dry nitrogen to separate the molecular sieves. Then, the two solvents were uniformly mixed with a shaking stirrer to form a cleaning solution composition, and then evaluated by the following evaluation methods. The results are shown in Table 1.
[0037] [Evaluation method]
[0038] Moisture content
[0039] Put the detergent composition of the present invention into a moisture content titrator (manufactured by Mettler, model E665), and then use Karl Fischer reagent SS (hereinafter referred to as KF reagent SS, titration equivalent = 0.7 ~ 1.0 mgH 2 O / milliliter) for titration, the water content of the detergent composition can be calculated by th...
Embodiment 2
[0052] Take 20 parts by weight of propylene glycol monomethyl ether (PGME) and 80 parts by weight of propylene glycol monomethyl ether acetate (PGMEA), and distill them with a distillation device (distillation conditions: heating to 110°C under normal pressure and maintaining for 1 hour) Cool to room temperature), then individually add molecular sieve 4A (granular), and stir for 6 hours for pretreatment. The weight ratio of molecular sieve to PGME or PGMEA is 2 / 100. Then, they were filtered under dry nitrogen. After separating the molecular sieves, the two solvents were uniformly mixed with a shaking stirrer to form a cleaning solution composition, and then evaluated by the above evaluation methods. The results are shown in Table 1.
Embodiment 3
[0054] The operation method is the same as that of Example 1, except that PGME and PGMEA are added to molecular sieve 4A (granular) and stirred for 12 hours for pretreatment, and then evaluated by the above evaluation methods. The results are shown in Table 1.
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