Fe-Ni base precipitation-strengthened austenite alloy and preparation method thereof

A precipitation strengthening and austenitic technology, which is applied in the field of Fe-Ni-based precipitation strengthening austenitic alloy and its preparation, can solve the problems of low hydrogen damage resistance, low strength, limited application range and influence, and achieve hydrogen resistance Improvement of damage performance and improvement of hydrogen damage resistance

Active Publication Date: 2011-06-08
INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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Problems solved by technology

[0002] Hydrogen energy is considered to be an important secondary energy source in the new century due to its clean combustion products, high combustion efficiency, and regeneration. The development and utilization of hydrogen energy has attracted widespread attention. However, in many harsh hydrogen environments, materials Problems such as damage and service life decline have been paid more and more attention by people.
Some single-phase austenitic alloys have good hydrogen resistance, but their low strength limits their application range
Fe-Ni based precipitation-strengthened austenitic alloys have high yield strength and good plasticity, and are widely used in harsh hydrogen-facing environments, but their resistance to hydrogen damage is significantly lower than that of single-phase austenitic alloys, which affects this type of alloy. Alloys are widely used in many fields as anti-hydrogen embrittlement materials, and the hydrogen damage resistance of alloys needs to be further improved

Method used

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  • Fe-Ni base precipitation-strengthened austenite alloy and preparation method thereof
  • Fe-Ni base precipitation-strengthened austenite alloy and preparation method thereof
  • Fe-Ni base precipitation-strengthened austenite alloy and preparation method thereof

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Embodiment 1

[0020] Conventional raw materials such as industrial pure iron, electrolytic nickel, sponge titanium, metal chromium, molybdenum, vanadium, aluminum and boron iron are used. The alloy composition is shown in Table 1.

[0021] Table 1 Chemical Composition of Alloys

[0022]

[0023] The specific production process steps are as follows:

[0024] 1) Put the above-mentioned raw materials into a CaO crucible, carry out vacuum induction melting, heat up for melting and casting, and after the ingot is completely solidified, open the mold and take it out;

[0025] 2) Homogenize the ingot at 1100-1180°C for 20 hours, then cool it with the furnace, and then perform surface grinding treatment to remove surface oxide scale;

[0026] 3) After holding at 1050-1150°C for 3-5 hours, alloy forging is carried out on a 750kg forging hammer. The billet forging temperature is 1100°C and the forging temperature is 950°C; and rolled into bars for optimum hydrogen resistance;

[0027] 4) The he...

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Abstract

The invention relates to the field of precipitation-strengthened austenite alloys, in particular to a Fe-Ni base precipitation-enhanced austenite alloy and a preparation method. The austenite alloy comprises the following elements in percentage by mass: 27 to 32 percent of nickel, 13 to 17 percent of chromium, 0.5 to 2 percent of molybdenum, 1.5 to 3 percent of titanium, 0.1 to 0.5 percent of aluminum, 0.1 to 0.6 percent of vanadium, 0.1 to 0.6 percent of silicon, 0.0005 to 0.02 percent of boron, less than 0.02 percent of carbon and the balance of iron and inevitable impurities. In the invention, the Fe-Ni alloy is taken as base, the content of the element boron in the alloy is improved, appropriate hot machining, and thermal treatment and hot hydrogen filling processes are performed, so that the crystal boundary precipitated phase of the alloy is controlled under a reasonable thermal treatment rule, and high mechanical property and high hydrogen damage resistance of a prepared alloy material are ensured. The precipitation-enhanced austenite alloy can be applied to hydrogen close environments of industries with high requirements such as aviation, nuclear energy, petrochemical industry and the like.

Description

Technical field: [0001] The invention relates to the field of precipitation-strengthened austenitic alloys, in particular to a Fe-Ni-based precipitation-strengthened austenitic alloy and a preparation method thereof. content, combined with certain thermal processing and heat treatment processes, can reduce the hydrogen damage of the alloy and improve the hydrogen damage resistance of the alloy. Background technique: [0002] Hydrogen energy is considered to be an important secondary energy source in the new century due to its clean combustion products, high combustion efficiency, and regeneration. The development and utilization of hydrogen energy has attracted widespread attention. However, in many harsh hydrogen environments, materials Problems such as damage and service life decline have been paid more and more attention by people. Some single-phase austenitic alloys have good hydrogen resistance, but their low strength limits their application range. Fe-Ni based precip...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C38/54C22C33/00
Inventor 戎利建郭子峰赵明久闫德胜姜海昌刘树伟李依依
Owner INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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