Composite armadillidium vulgare extract and preparation method and application thereof to pain relieving medicaments
A technology of compound sarcophagus and extract, which is applied in the field of compound sarcophagus extract and its preparation, and can solve the problems of not being easy to use, adverse reactions of the cardiovascular system, improper dosage control, etc.
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Embodiment 1
[0089] Ratwort, Corydalis Corydalis and Xu Changqing Compound Extract
[0090]Take 1 kg of Corydalis Corydalis, 1 kg of Corydalis Corydalis, and 1 kg of Xu Changqing, mix the above-mentioned Corydalis Corydalis and Xu Changqing, add 10 kg of water, extract 3 times at 100 ° C, 1.5 hours each time, and combine the extracts; take the above Corydal Corydalis, add 4 times the amount of 70 % ethanol, heated and refluxed for 3 times, each time for 1h, the extract was filtered, and the filtrate was collected. Combine the filtrates, concentrate to 10% of the original volume, add 95% ethanol to make the ethanol concentration 60%, precipitate, take the supernatant, concentrate and recover the ethanol, spray dry the extract to obtain a dry powder.
Embodiment 2
[0092] Alcohol Extract of Ratwort, Corydalis Corydalis, Xu Changqing Compound
[0093] Weighing mouse woman: 1kg, Yanhusuo: 0.8kg, Xu Changqing: 0.7kg
[0094] Mix the above-mentioned fenugreek, Corydalis Corydalis, and Xu Changqing, add 12 times the weight of 80% ethanol, reflux extraction for 3 times, each time for 1 hour, and combine the extracts. Concentrate under reduced pressure to obtain the ethanol extracts of the compound recipe of sarcocarpus, Corydalis Corydalis and Xu Changqing.
Embodiment 3
[0096] Ratwort, Corydalis Corydalis and Xu Changqing Compound Extract
[0097] Take 1 kg of Corydalis 1 kg, 0.7 kg of Corydalis Corydalis, and 1 kg of Xu Changqing, mix the above-mentioned Corydalis Corydalis and Xu Changqing, add 15 kg of water, extract 3 times at 100 ° C, 2.0 hours each time, and combine the extracts; 70% ethanol, heated and refluxed for 3 times, 1 hour each time, filtered the extract, and collected the filtrate. Combine the filtrates, concentrate to 10% of the original volume, add 95% ethanol to make the ethanol concentration 60%, precipitate, take the supernatant, concentrate and recover the ethanol, spray dry the extract to obtain a dry powder.
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