A kind of preparation method of compound Chinese medicine lotion
A technology of compound traditional Chinese medicine and lotion, applied in the field of daily necessities, can solve the problems such as difficulty in realizing the disinfection function of chlorine-containing detergents, strong corrosiveness, poor stability, etc., and achieve the effects of low cost, high safety and fragrant smell.
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Embodiment 1
[0041] The ratio of compound medicinal materials is 6:3:3:3:3:2:1, that is, according to the ratio of Sophora flavescens 30g, Zihua Diding 15g, Folium Folium 15g, Cnidium 15g, Dandelion 15g, Eucommia 10g, Ginkgo biloba 5g Weigh the medicinal materials, add water to submerge the medicinal materials by 3-5cm, and soak. Adjust the pH of the medicinal material and water mixture to 4.5 with dilute hydrochloric acid, and add 1.67×10 -4 g cellulase and 0.5 x 10 -4 Add the two enzymes at a ratio of g pectinase, stir evenly, and enzymolyze in a water bath at 50°C for 3 hours.
[0042] The enzymatic hydrolyzate was extracted with water, adding water 8, 7, and 6 times the weight of the raw material dry medicinal material for three extractions, extracting at 90°C for 1 hour, filtering respectively, and combining the filtrates. Centrifuge at 3000r / min for 20min, and take the supernatant. The supernatant was precipitated with 75% ethanol for 24 hours, and the supernatant was concentrated...
Embodiment 2
[0044] The ratio of compound medicinal materials is 6:6:3:3:3:1:1, that is, according to the ratio of 30g Sophora flavescens, 30g Zihua Diding, 15g Folium Folium, 15g Cnidium Fructus, 15g Dandelion, 5g Eucommia Leaf, and 5g Ginkgo Leaf Weigh the medicinal materials, add water to submerge the medicinal materials by 3-5cm, and soak. Adjust the pH of the medicinal material and water mixture to 5 with dilute hydrochloric acid, and add 2.2×10 -4 g cellulase and 0.9 x 10 -4 The ratio of g pectinase was added to the two enzymes, stirred evenly, and enzymatically hydrolyzed in a water bath at 52°C for 2.5 hours.
[0045] The enzymatic hydrolyzate was extracted with water, adding water 7, 6, and 4 times the weight of the raw material dry medicinal material for three extractions, extracting at 85°C for 1 hour, filtering respectively, and combining the filtrates. Centrifuge at 3000r / min for 20min, and take the supernatant. The supernatant was precipitated with 75 volume % ethanol for ...
Embodiment 3
[0047] The ratio of compound medicinal materials is 6:5:4:3:2:1:1, that is, according to the ratio of 30g of Sophora flavescens, 25g of Zihua Diding, 20g of Folium Folium, 15g of Fructus Cnidii, 10g of Dandelion, 5g of Eucommia Leaf, and 5g of Ginkgo Leaf Weigh the medicinal materials, add water to submerge the medicinal materials by 3-5cm, and soak. Adjust the pH of the medicinal material and water mixture to 4.8 with dilute hydrochloric acid, and add 2.0×10 -4 g cellulase and 0.6 x 10 -4 The ratio of g pectinase was added to the two enzymes, stirred evenly, and enzymatically hydrolyzed in a water bath at 52°C for 2.5 hours.
[0048] The enzymatic hydrolyzate was extracted with water, and water 8, 5, and 5 times the weight of the raw material dry medicinal material was added to the three extractions, extracted at 87°C for 1 hour, and the filtrates were combined after filtration. Centrifuge at 3000r / min for 20min, and take the supernatant. The supernatant was precipitated w...
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