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Solid phase synthesis method of silver and chitosan and/or chitosan derivative nanometer compound

A technology of chitosan derivatives and nanocomposites, which is applied in the field of solid-phase synthesis of silver, chitosan and/or its derivative nanocomposites, can solve problems such as preparation methods and applications that have not been reported, and achieves Uniform particle size effect

Inactive Publication Date: 2012-02-22
LIAOCHENG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The preparation method and application of silver-chitosan and its derivatives nanocomposite powder with chitosan and its derivatives as carrier, dispersant and protective agent have not been reported

Method used

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  • Solid phase synthesis method of silver and chitosan and/or chitosan derivative nanometer compound
  • Solid phase synthesis method of silver and chitosan and/or chitosan derivative nanometer compound

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0054] A kind of silver, chitosan nanocomposite, preparation method step is as follows:

[0055] (1) Grind 10g chitosan into fine powder;

[0056] (2) Grinding 0.005g of silver nitrate into fine powder;

[0057] (3) Mix chitosan fine powder and silver nitrate fine powder, and grind thoroughly for 1 hour;

[0058] (4) Add 0.005 g of ascorbic acid, and continue to fully grind for 2 hours to obtain a silver-chitosan nanocomposite (sample 1) with a silver particle size of 1-100 nm.

Embodiment 2

[0060] A nanocomposite of silver and chitosan derivatives, the preparation method steps are as follows:

[0061] (1) Grinding 10g carboxymethyl chitosan into fine powder;

[0062] (2) Grinding 0.005g of silver nitrate into fine powder;

[0063] (3) Mix carboxymethyl chitosan fine powder with silver nitrate fine powder and grind them thoroughly for 2 hours;

[0064] (4) Add 0.005 g of glucose and continue to grind thoroughly for 2.5 hours to obtain a silver-chitosan derivative nanocomposite (sample 2) with a silver particle size of 1-100 nm.

Embodiment 3

[0066] A nanocomposite of silver, chitosan and chitosan derivatives, the preparation method steps are as follows:

[0067] (1) Grind 7g chitosan and 3g hydroxypropyl chitosan into fine powder;

[0068] (2) Grinding 0.005g of silver nitrate into fine powder;

[0069] (3) Mix chitosan and hydroxypropyl chitosan fine powder with silver nitrate fine powder, and fully grind for 2 hours;

[0070] (4) Add 0.005 g of N-acetylglucosamine, and continue to fully grind for 6 hours to obtain silver, chitosan and chitosan derivative nanocomposites with a silver particle size of 1-100 nm.

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Abstract

The invention discloses a solid phase synthesis method of a silver and chitosan and / or chitosan derivative nanometer compound. The silver and chitosan and / or chitosan derivative nanometer compound has the effects of promoting wound healing, stopping bleeding, relieving pain, diminishing inflammation and killing bacteria. The silver and chitosan and / or chitosan derivative nanometer compound can beutilized for treating female colpitis, cervicitis, cervical erosion, bedsore, skin ulcers, burns, scalds, wounds, other skin inflammation, tinea manus and tinea pedis. The silver and chitosan and / or chitosan derivative nanometer compound also can be utilized for preparation of various wound dressings such as films, sponges, suppositories for gynaecology, and adhesive films.

Description

[0001] This application is a divisional application: original application number: 200910017600.8, filing date: 2009.8.11, invention name: preparation method and application of nanocomposite of silver, chitosan and / or its derivatives. technical field [0002] The invention relates to the technical fields of chemical industry and medicine, in particular to a preparation method of silver, chitosan and / or chitosan derivative nanocomposite powder and its application in the treatment of female vaginitis, cervicitis, cervical erosion, bedsore, skin Ulcers, burns, scalds, wounds, and other skin inflammations, tinea pedis and other pharmaceutical applications, and can also be used to prepare various trauma dressings such as films, sponges, gynecological suppositories, films, etc. Background technique [0003] Chitosan is the deacetylation product of chitin, and it is a basic amino polysaccharide existing in nature. In recent years, studies by scholars at home and abroad have shown th...

Claims

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Application Information

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IPC IPC(8): C08L5/08C08K3/08B22F9/20
Inventor 桑青秦东风
Owner LIAOCHENG UNIV
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