Method for producing polyformaldehyde dimethyl ether
A technology of polyoxymethylene dimethyl ether and trioxymethylene, which is applied in chemical instruments and methods, preparation of organic compounds, sustainable manufacturing/processing, etc., can solve the problem of low selectivity, etc. Facilitates responses and overcomes difficult-to-control effects
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Embodiment 1
[0014] according to figure 1 As shown, the operating pressure of the catalytic distillation column is 0.5MPa, the theoretical plate number of the stripping section is 20, the separation efficiency of the catalytic reaction section is equivalent to the theoretical plate number of 25, the catalyst is SAPO-34 molecular sieve, and the flow rate of trioxymethylene is 3 g / min. Enter the first theoretical plate (counting from top to bottom, the same below), methanol enters from the bottom of the catalytic reaction section at a flow rate of 1 g / min, the ratio of the first part of the tower to the second part of the material is 7:1, and the effective reaction conditions The temperature range of the catalytic reaction section is 110 to 130 ° C, and the bottom of the tower is extracted at a flow rate of 4 g / min. The results of catalytic distillation are shown in Table 1.
Embodiment 2~5
[0016] Other conditions are the same as in Example 1, except that the type of catalyst is changed. The catalysts are Suqing brand 001×4 strong acid resin, ZSM-5, SO 4 -2 / Fe 2 O 3 , Cl -1 / TiO 2 and SO 4 -2 / Fe 2 O 3 , the catalytic distillation results are shown in Table 1.
Embodiment 6
[0018] according to figure 1 As shown, the operating pressure of the catalytic distillation column is 4.0 MPa, the number of theoretical plates in the stripping section is 5, the separation efficiency of the catalytic reaction section is equivalent to 5 theoretical plates, the catalyst is MCM-22 molecular sieve, and the flow rate of trioxymethylene is 1 g / min. and methanol into the first theoretical plate at a flow rate of 5 g / min, the ratio of the first part of the tower to the second part of the material is 15:1, the temperature range of the catalytic reaction section of the effective reaction conditions is 180 ~ 200 ℃, the bottom of the tower is 21 The flow rate of g / min is extracted, and the results of catalytic distillation are shown in Table 1.
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