Ferrite absorber for absorbing high-order mode of high-frequency cavity and preparation method thereof
A ferrite and high-frequency cavity technology, applied in the field of ferrite absorber and its preparation, can solve problems such as affecting beam stability and beam oscillation loss, so as to improve stability, prevent performance deterioration, and avoid changes Effect
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Embodiment example 1
[0034] The ferrite powder is prepared by the powder solid state reaction method of the present invention, and the ferrite powder has a molecular chemical formula of Ni 0.4 Zn 0.4 co 0.2 Fe 2 o 4 ferrite powder. Among them, respectively weigh 3194.0g Fe 2 o 3 , 597.6g NiO, 651.0g ZnO and 299.7g CoO raw powder, mixed and sieved the raw powder by ball milling to obtain 4740g of mixed powder. The sieved powder was put into a muffle furnace for pre-sintering at 950°C for 2h. Then complete the preparation of the ferrite absorber according to the subsequent steps (2)-(6) in the technical solution of the present invention. Among them, the sintered powder is treated in the ball mill mixer for 4 hours for the second ball milling; 5wt% PVA aqueous solution is used as the forming agent; the weight ratio of ferrite powder: forming agent = 100:5 is mixed and granulated, and pressed Form a cylindrical ferrite body; raise the temperature in the air at a rate of 0.8°C / min, and keep the...
Embodiment example 2
[0037] The ferrite powder is prepared by the powder solid state reaction method of the present invention, and the ferrite powder has a molecular chemical formula of Ni 0.6 Zn 0.3 co 0.1 Fe 2 o 4 ferrite powder. Among them, respectively weigh 3194.0g Fe 2 o 3 , 896.4g NiO, 488.3g ZnO and 149.9g CoO raw powder, mixed and sieved the raw powder by ball milling to obtain 4725g of mixed powder. The sieved powder was put into a muffle furnace for pre-sintering at 900°C for 2h. Then complete the preparation of the ferrite absorber according to steps (2) to (6) in the technical solution of the present invention. Among them, the sintered powder is treated in the ball mill mixer for 5h for the second ball milling; 6wt% PVA aqueous solution is used as the forming agent; according to the weight ratio of ferrite powder:forming agent=105:10, it is mixed and granulated, and pressed Form a cylindrical ferrite green body; heat up at a rate of 0.5°C / min in the air, and hold at 400°C for ...
Embodiment example 3
[0040] The ferrite powder is prepared by the pipeline synthetic chemical co-precipitation method. The ferrite powder has the molecular chemical formula of Ni 0.8 Zn 0.16 co 0.04 Fe 2 o 4 ferrite powder. Among them, 4.0L of reaction mother liquor with a metal ion concentration of 1.5mol / L, 15wt% NH 3 ·H 2 2.8L of O solution and about 1.0mL of 15wt% NaOH solution, then prepare a reaction solution with a pH of 10 and heat it to 60°C; 4 + The molar ratio of metal ions is 2:1 to control the metal ion reaction mother liquor and NH 3 ·H 2 O flow, adjust the NaOH flow at the same time, control the pH of the reaction to be about 10, and the amount of NaOH solution after the reaction is about 0.2mL; quickly dry the reactant at 150°C to obtain about 450g of ferrite powder. The ferrite powder was prepared 10 times in the same way, and the total amount of ferrite powder obtained was about 4500 g. The sieved powder was put into a muffle furnace for pre-sintering at 700°C for 2h. ...
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