Synthesis of thickening agent for methanol-based fracturing fluid
A methanol-based, thickening agent technology, applied in the direction of drilling compositions, chemical instruments and methods, etc., can solve the problems of low viscosity retention, poor shear resistance, poor temperature resistance, etc., and achieve dissolution speed Fast, good temperature and shear resistance
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[0022] The weight percent of each monomer and water: AM: DMC: AN: AMPS: DMAM: H 2 O=5:25:3:3:3:61.
[0023] Solution preparation: Add 610g of distilled water into a 2000ml beaker, add 50g of AM monomer, add 250g of DMC monomer, 30g of AN monomer, add 30g of AMPS monomer, add 30g of DMAM monomer, stir and dissolve for 30 minutes, under stirring conditions Slowly add neutralizer (sodium hydroxide) to pH 6.5. The stirring solution was continued to ripen for 30 minutes.
[0024] Solution adjustment: adjust the pH value to 6.5±0.5 again, and adjust the temperature to 15±1°C.
[0025] Polymerization of the solution: Blow nitrogen to remove oxygen for 20 minutes, add catalysts V650.5g / L, V500.05g / L, ammonium persulfate 0.03g / L, sodium formaldehyde sulfoxylate 0.03g / L sequentially under nitrogen protection, stop Blow nitrogen and seal the polymerization tank, induce for 15-20 minutes, and observe whether there is a temperature rise. When there is a temperature rise of 2°C during th...
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