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Alkaline corrosive agent for representing defects in GaN (Gallium Nitride) epitaxial layer and preparation method thereof

A technology of etchant and epitaxial layer, which is applied in the field of alkaline etchant and preparation for characterizing defects in GaN epitaxial layer, can solve the problems of difficult preparation of GaN bulk single crystal, difficulty in obtaining high-quality GaN bulk single crystal material, etc., to achieve strong practicability, Ease of operation and the effect of accelerating the corrosion rate

Inactive Publication Date: 2012-06-13
HEBEI UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the preparation of GaN bulk single crystal is difficult, and it is difficult to obtain GaN bulk single crystal material with good quality and large size as a substrate, so the epitaxial growth of GaN is usually carried out in the form of hetero-epitaxy
Due to the lattice mismatch and thermal mismatch between the substrate material and the GaN epitaxial layer, many hexagonal grains are formed during the growth process, and these individual grains are tilted and rotated in the GaN epitaxial layer, resulting in a high density of defects

Method used

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  • Alkaline corrosive agent for representing defects in GaN (Gallium Nitride) epitaxial layer and preparation method thereof
  • Alkaline corrosive agent for representing defects in GaN (Gallium Nitride) epitaxial layer and preparation method thereof
  • Alkaline corrosive agent for representing defects in GaN (Gallium Nitride) epitaxial layer and preparation method thereof

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Embodiment Construction

[0017] The present invention will be further described below in conjunction with the embodiments and accompanying drawings.

[0018] The alkaline etchant (alkaline etchant) for characterizing defects in GaN epitaxial layer designed by the present invention is characterized in that the alkaline etchant is mixed with two kinds of strong alkalis KOH:NaOH in a mass ratio of 2:1-1:2 Uniform, used for wet chemical etching of GaN materials.

[0019] The preparation method of the alkaline corrosive agent of the present invention is: first put the granular two kinds of strong alkalis NaOH and KOH on weighing paper respectively, and weigh the two kinds of strong alkalis according to the mass ratio; Put the two kinds of strong alkalis that have been measured into a nickel crucible and mix them evenly.

[0020] In the preparation method of the alkaline etchant of the present invention, the procedures themselves are all prior art. The preparation method of the invention has the advantage...

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Abstract

The invention discloses an alkaline corrosive agent for representing defects in a GaN (Gallium Nitride) epitaxial layer and a preparation method thereof. The alkaline corrosive agent is characterized by being prepared through uniformly mixing two types of strong bases, namely KOH and NaOH at the mass ratio of (1-2):(2-1), and being used for wet-method chemical corrosion of a GaN material. The preparation method comprises the following steps of: firstly, respectively placing two types of granular strong bases, namely KOH and NaOH on weighing paper and respectively weighing the two types of strong bases according to the mass ratio; and then putting the two types of strong bases, which are weighed according to the mass ratio, into a nickel crucible and uniformly mixing to obtain the alkaline corrosive agent.

Description

technical field [0001] The invention relates to chemical etching technology, in particular to an alkaline etchant for characterizing defects in GaN epitaxial layers and a preparation method. Background technique [0002] In recent years, Group III nitride semiconductor materials represented by GaN are very suitable for the production of high-power, radiation-resistant, high-frequency and high-density integrated electronic devices, as well as blue and green light due to their chemical properties of high temperature resistance and corrosion resistance. And ultraviolet optoelectronic devices have become a research hotspot worldwide. However, it is difficult to prepare GaN bulk single crystals, and it is difficult to obtain GaN bulk single crystals with good quality and large size as substrates, so the epitaxial growth of GaN is usually carried out in the form of heteroepitaxial growth. Due to the lattice mismatch and thermal mismatch between the substrate material and the GaN ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/32G01N23/22
Inventor 田园刘彩池郝秋艳解新建张昆
Owner HEBEI UNIV OF TECH