3results about How to "Suitable for industrial implementation" patented technology

The invention provides a liquid red direct dye and a preparation method thereof, and the method comprises the following steps: S1, dispersing 2-amino-5-naphthol-7-sulfonic acid and bis (trichloromethyl) carbonate in water, adjusting the pH value of a reaction system by using a first organic base, and reacting to obtain a scarlet acid aqueous solution; s2, dispersing a sulfo aromatic amine compound and nitrite in water, adjusting the pH value of a reaction system by using inorganic acid, reacting to obtain sulfo aromatic amine diazonium salt precipitate, and performing solid-liquid separation to obtain sulfo aromatic amine diazonium salt; and S3, adding the sulfonic aromatic amine diazonium salt in the step S2 into the scarlet acid aqueous solution in the step S1, adjusting the pH value of the reaction system by using second organic alkali, and reacting to obtain the liquid red direct dye. Through the preparation method, the red direct dye which can stably exist in a liquid form and is suitable for direct use can be obtained.

The application discloses a method for preparing adipic acid by coupling hydrogen production through electro-catalytic oxidation of cyclohexanol / cyclohexanone. The H-shaped electrolytic tank is used for catalytic oxidation; the working electrode of the anode chamber and the cathode chamber and the reference electrode jointly form an electro-catalytic reactor; the reaction raw material liquid is a water solution of cyclohexanol / cyclohexanone and electrolyte, and the anode is oxidized into adipic acid and hydrogen is generated in the cathode under a certain working voltage and current density after reaction for a period of time. Compared with the traditional process, the application has the advantages of high efficiency, high selectivity, green, low cost, simple operation and the like, is suitable for industrial implementation, and has a wide application prospect.

The present application relates to the technical field of organic small molecule material detection, in particular to a fluorescent molecular probe with double-dynamic monitoring function and a preparation method and application thereof. ‑ In DMF-water solution, the molecular probe presents a double-excitation-double-emission fluorescence with the increase of ClO ‑ concentration, and the fluorescence intensity presents a "on-off-on" double-transition dynamic detection response with the change of acid-base environment, which endows the molecular probe with double-dynamic monitoring function for ClO ‑ and the change of acid-base environment. ‑ The binary system has fluorescence emission "on-off" detection performance; and the detection is fast and sensitive. The molecular probe provided by the present application has the advantages of mild synthesis condition and simple preparation, which creates favorable conditions for its popularization and application.