Preparation method of pericarpium citri reticulatae absolute oil and application of pericarpium citri reticulatae absolute oil in cigarettes

A technology of tangerine peel and tobacco materials, applied in the fields of application, tobacco, and tobacco treatment, to achieve the effects of improving quality, high yield, solution state, and solubility

Inactive Publication Date: 2016-12-14
YUNNAN YANGRUI TECH GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

On the other hand, at the present stage, because of the pharmacological effects of tangerine peel, domestic research on the application of tangerine peel is mainly concentrated in the field of medicine and health care, with less application in other aspects, and even less application in cigarettes

Method used

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  • Preparation method of pericarpium citri reticulatae absolute oil and application of pericarpium citri reticulatae absolute oil in cigarettes

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] (1) Crush tangerine peel: crush tangerine peel with a water content of 10% to 5mm tangerine peel grains;

[0030] (2) Fermentation of tangerine peel: take pectinase according to 1.5% of the mass of tangerine peel grains, and take cellulase according to 1.5% of the mass of tangerine peel grains; place the tangerine peel grains obtained in step (1) at a temperature of 301°C and a humidity of 65%. In a constant temperature and humidity environment, add pectinase and cellulase to ferment for 3 days by spraying, and turn the pile every 1 to 2 days to fully decompose the pectin and cellulose in the tangerine peel;

[0031] (3) Dried tangerine peel: Add 10 times the volume of petroleum ether to the fermented tangerine peel grains obtained in step (2) and mix well to obtain a mixed material;

[0032] (4) Extraction and filtration: Heat the mixed material obtained in step (3) to 100°C and keep it warm for 5 hours, then filter with a 100-mesh filter to obtain the extract;

[003...

Embodiment 2

[0038] (1) Crush tangerine peel: crush tangerine peel with a water content of 20% to tangerine peel grains with a particle size of 4mm;

[0039] (2) Fermentation of tangerine peel: take pectinase according to 5% of the weight of tangerine peel grains, and take cellulase according to 5% of the weight of tangerine peel grains; place the dried tangerine peel grains obtained in step (1) at a temperature of 40°C and a humidity of 90%. In a constant temperature and humidity environment, add pectinase and cellulase to ferment for 10 days by spraying, and turn the pile every 1 to 2 days to fully decompose the pectin and cellulose in the tangerine peel;

[0040] (3) Dried tangerine peel: Add 2 times the volume of petroleum ether to the fermented tangerine peel grains obtained in step (2) and mix well to obtain a mixed material;

[0041] (4) Extraction and filtration: Heat the mixed material obtained in step (3) to 30°C and keep it warm for 12 hours, then filter with a 10-mesh filter to...

Embodiment 3

[0047] (1) Crush tangerine peel: crush tangerine peel with a water content of 7% to 0.1mm tangerine peel grains;

[0048](2) Fermentation of tangerine peel: take pectinase according to 0.1% of the mass of tangerine peel grains, and take cellulase according to 0.1% of the mass of tangerine peel grains; place the tangerine peel grains obtained in step (1) in a room with a temperature of 60°C and a humidity of 60%. In a constant temperature and humidity environment, add pectinase and cellulase to ferment for 1 day by spraying, and turn the pile every 1 to 2 days to fully decompose the pectin and cellulose in the tangerine peel;

[0049] (3) Dried tangerine peel: Add 15 times the volume of petroleum ether to the fermented tangerine peel grains obtained in step (2) and mix well to obtain a mixed material;

[0050] (4) Extraction and filtration: Heat the mixed material obtained in step (3) to 150°C and keep it warm for 0.5h, then filter with a 1000-mesh filter to obtain the extract;...

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Abstract

The invention discloses a preparation method of pericarpium citri reticulatae absolute oil. The pericarpium citri reticulatae absolute oil is obtained through the steps of pericarpium citri reticulatae crushing, pericarpium citri reticulatae fermenting, pericarpium citri reticulatae extracting, extracting and filtering, concentrating, alcohol precipitating and concentrating. According to the obtain pericarpium citri reticulatae absolute oil, the content of flavonoids such as hesperidin, nobiletin and tangeretin and the content of volatile oil such as limonene are high, therefore, the unique aroma of pericarpium citri reticulatae is effectively kept, and the natural flavor is clearer when the pericarpium citri reticulatae absolute oil is applied to the cigarettes; in addition, the application range of the absolute oil can be wider, the state and solubility problems of a pericarpium citri reticulatae extract are solved, and the absolute oil can be better applied to the cigarettes; the preparation process is simple, the operability is high, the whole production process is efficient, and the method is suitable for industrialized implementation; on the other hand, when the pericarpium citri reticulatae absolute oil prepared through the method is applied to the cigarettes, the mouthfeel and the aftertaste of cigarette smoking can be improved, the special natural flavor can be given to the cigarettes, and the smoke quality can be promoted.

Description

technical field [0001] The invention relates to the technical field of plant extraction and its application, in particular to a preparation method of tangerine peel absolute and its application in cigarettes. Background technique [0002] Chenpi, the name of traditional Chinese medicine. It is also called orange peel, expensive old peel, red peel, yellow orange peel, wide orange peel, Xinhui peel, orange peel, and wide tangerine peel. It is the mature pericarp of Rutaceae plant Tangerine and its cultivars, the fruit is picked off, the pericarp is peeled off, and dried in the shade or ventilated. The peel is named after Chen Zheliang. Tangerine peel has a bitter taste and warm nature. It has the effects of warming the stomach and dispelling cold, regulating qi and invigorating the spleen. It is suitable for people with symptoms such as full stomach, indigestion, loss of appetite, and cough with phlegm. [0003] Tangerine peel has the effects of regulating qi and appetizing...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02A24B15/30
CPCC11B9/025A24B15/303
Inventor 姚国娇邹由郭剑梁正进温光和杨雪燕
Owner YUNNAN YANGRUI TECH GRP
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