Fiber screen bag and method for rapidly determining coarse fiber
A rapid measurement and screen bag technology, applied in the direction of weighing by removing certain components, can solve the problems of slow operation process, low efficiency, long time, etc., achieve high precision and accuracy, and accurate analysis results , Analyze the effect of cost reduction
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Embodiment 1
[0028] 1. Reagents, instruments and equipment:
[0029] (1) Sulfuric acid solution: c(H 2 SO 4 )=0.13mol / L. Each 1000ml contains 12.5g (about 7.10ml) of sulfuric acid.
[0030] (2) Potassium hydroxide solution: c(KOH)=0.23mol / L. Each 1000ml contains 12.5g of potassium hydroxide.
[0031] (3) Acetone.
[0032] (4) Special fiber screen bag (the screen aperture is 25um).
[0033] (5) Crushing equipment: it can crush the sample so that it can completely pass through a sieve with a sieve hole of 1mm.
[0034] (6) Analytical balance: Sensitivity 0.1mg.
[0035] (7) Beaker: capacity 2000ml or with a suitable cooling device, such as a condenser or a pan.
[0036] (8) Drying box: It is heated by electricity, can be ventilated, and can maintain temperature.
[0037] (9) Desiccator: filled with blue silica gel desiccant, inside a porous plate with a thickness of 2mm, preferably made of aluminum or stainless ste...
Embodiment 2
[0058] Choose 8 empty fiber screen bags to process according to the method and steps of the present invention, and measure the weight loss of the screen bags after acid, alkali and acetone treatment of the empty bags and drying in a 105°C oven for 1h. The results are shown in Table 2 , the average weight loss is 0.0005g, basically zero, which meets the experimental requirements. Another 4 empty fiber screen bags were selected and burned at 500°C for 30 minutes to measure the ash weight. The results are shown in Table 3. The average ash weight of each bag was -0.0004g, basically zero, which met the experimental requirements.
[0059]
[0060] Table 2 The drying quality change results of fiber mesh bags treated with acid, alkali and acetone
[0061] empty bag number Empty screen bag weight (g) Drying bag weight (g) weight loss(g) 1 0.2252 0.2249 0.0003 2 0.2376 0.2375 0.0001 3 0.2302 0.2296 0.0006 4 0.2168 0.2166 0.0002 5 0.226...
Embodiment 3
[0065] Select 6 samples of powder, wheat bran, feed, rabbit compound feed, soybean meal, and grass powder, and each sample is made into 5 parallel samples, and the crude fiber content is measured according to the method and steps of the present invention. The results of the measured samples are shown in Table 4, It can be seen that the results of parallel samples are relatively close, and the relative standard deviation (RSD) is basically within 5%. The precision calculation results are shown in Table 5, and the precision is relatively high.
[0066] Table 4 Results of sample precision determination by fiber mesh bags Unit: %
[0067] Parallel number Second powder Wheat bran feed soybean meal rabbit feed grass powder 1 5.54 10.64 11.66 4.17 12.23 32.94 2 5.61 10.81 11.70 4.36 12.24 33.06 3 5.67 11.12 12.07 4.79 12.82 34.78 4 5.86 11.14 12.17 4.92 13.33 34.90 5 5.99 11.16 12.51 5.05 13.43 36.53 RSD (...
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