Refining process of o-nitrophenol
A technology of o-nitrophenol and process, applied in the field of refining process of o-nitrophenol, can solve the problems of high COD of waste water, high energy consumption, intractable treatment and recycling, etc., save energy and equipment, reduce production cost, The effect of reducing the impurity content
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[0023] Below in conjunction with embodiment, the present invention is further described.
[0024] The refining process of o-nitrophenol comprises the steps:
[0025] ①. Pour the methyl ether oxidation reaction mother liquid water into the storage tank, and use the condenser to circulate and cool down, and the temperature drops below 30°C;
[0026] ②, let stand for 1 hour (the stratification is more obvious), pour the middle and upper layer water into the decolorization pot; the lower layer material can be returned to the oxidation system, and o-nitroanisole is recovered;
[0027] ③. Add 1% powdered activated carbon to the decolorization pot, heat up to 60°C, and decolorize for 1 hour;
[0028] 4. After the decolorization is qualified (indicators such as detection of chroma), the decolorization liquid is filtered through a filter press, and the filter residue activated carbon is extracted with methanol to extract o-nitroanisole, and the activated carbon is recovered and reused...
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