Bicomponent transparent finishing fire retardant coating and preparation method thereof
A fire retardant coating, two-component technology, applied in the direction of fire retardant coatings, coatings, etc., can solve the problems of poor coating film flexibility, coating film cracking, etc., and achieve the effects of low cost, loose reaction conditions, and simple and easy preparation methods.
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Embodiment 1
[0034] (1) Add 25g of pentaerythritol, 50g of polyphosphoric acid, and 25g of PEG200 into the reaction kettle, and heat up to melt the reactants. After the reactant is completely melted, start stirring to react, the reaction temperature is 100°C, and the reaction time is 4h, to obtain grafted polyphosphate; the prepared graft polyphosphate is made into a 50% aqueous solution, which is formazan Component.
[0035] (2) Weigh 400g of water-based hexamethylolmelamine formaldehyde resin (synthesized in the laboratory), which is component B.
[0036] (3) Blend and stir the above two components A and B for 30 minutes. After the stirring is completed, wait for the air bubbles in the coating to dissipate naturally, which is a two-component transparent decorative fireproof coating.
Embodiment 2
[0038] (1) Add 40g of pentaerythritol, 40g of polyphosphoric acid, and 20g of PEG300 into the reaction kettle, and heat up to melt the reactants. After the reactants are completely melted, start stirring to react, the reaction temperature is 120°C, and the reaction time is 5 hours to obtain grafted polyphosphate; the obtained graft polyphosphate is made into a 50% aqueous solution, which is formazan Component.
[0039] (2) Weigh 400g of water-based hexamethylolmelamine formaldehyde resin (synthesized in the laboratory), which is component B.
[0040] (3) Blend and stir the above two components A and B for 30 minutes. After the stirring is completed, wait for the air bubbles in the coating to dissipate naturally, which is a two-component transparent decorative fireproof coating.
Embodiment 3
[0042] (1) Add 32.5g of pentaerythritol, 45g of polyphosphoric acid, and 22.5g of PEG400 into the reaction kettle, and heat up to melt the reactants. After the reactants are completely melted, start stirring to react, and the reaction temperature is 110°C.
[0043] The reaction time is 4.5h, and the grafted polyphosphate is obtained; the prepared grafted polyphosphate is made into a 50% aqueous solution, which is the first component.
[0044] (2) Weigh 400g of water-based hexamethylolmelamine formaldehyde resin (synthesized in the laboratory), which is component B.
[0045] (3) Blend and stir the above two components A and B for 30 minutes. After the stirring is completed, wait for the air bubbles in the coating to dissipate naturally, which is a two-component transparent decorative fireproof coating.
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