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External sarcandra glabra ointment and preparation method thereof

A technology for external application of ointment and rheumatoid arthritis, which is applied in the directions of delivery of medical preparations containing active ingredients, anti-inflammatory agents, and ointments, and achieves significant economic and social benefits and simple preparation methods.

Inactive Publication Date: 2012-10-17
FUJIAN UNIV OF TRADITIONAL CHINESE MEDICINE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, according to the Chinese Pharmacopoeia and drug standards issued by the Ministry, there are no external medicines for Jiujie tea or swollen joint wind

Method used

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  • External sarcandra glabra ointment and preparation method thereof
  • External sarcandra glabra ointment and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] (1) Take sargassum and add water to decoct twice (the first water mass volume ratio is 1:10, the second: 1:6), each time for 1 hour, combine the decoction, filter, and the filtrate is concentrated to 70°C. Density is 1.02, natural cooling;

[0014] (2) Precipitate with 1ml of ethanol per gram of concentrated solution, and place overnight at room temperature;

[0015] (3) Aspirate the supernatant to recover ethanol and concentrate to a clear paste with a relative density of 1.05 at 70°C;

[0016] (4) Add 0.5 g of oil-in-water (O / W) emulsion matrix containing 0.6% borneol to each gram of clear ointment to prepare an ointment for external use. Specifically: Heat stearic acid and stearyl alcohol to melt, add liquid paraffin, etc., and stir to form an oil phase; add glycerin, Tween-80, potassium sorbate, and the above clear ointment at the same temperature (80-90°C) while stirring In the water phase of the composition; add borneol at about 60°C, stir continuously, cool, fi...

Embodiment 2

[0018] (1) Take sarcophagus and add water to decoct twice (the mass volume ratio of sarcophagus to water is 1:10), each time for 2 hours, combine the decoction, filter, and concentrate the filtrate to 70°C with a relative density of 1.10, naturally cool down;

[0019] (2) Precipitate with 2ml of ethanol per gram of concentrated solution, and place at room temperature for 24 hours;

[0020] (3) Take the supernatant and filter it, recover the ethanol from the filtrate and concentrate it to a clear cream with a relative density of 1.15 at 70°C, add 2 times the amount of oil-in-water (O / W) emulsion matrix containing 3% borneol, and make it for external use ointment. Specifically: Mix the oil phase ingredients (glyceryl monostearate, stearic acid, liquid paraffin, white petrolatum) and the water phase ingredients (triethanolamine, ethylparaben and the above clear ointment) respectively, and heat to 75-80 ℃, add the oil phase to the water phase, keep stirring, add borneol at about...

Embodiment 3

[0022] (1) Take sargassum and add water to decoct 3 times (mass volume ratio of sarcophagus to water is 1:12), each time for 3 hours, combine the decoction, filter, and concentrate the filtrate to 70°C with a relative density of 1.22, naturally cool down;

[0023] (2) Add 5ml of ethanol to each gram of concentrated solution, stir, let stand for refrigerated (temperature 2-10°C) for 10 hours, separate the supernatant and filter; add 1ml of 80% ethanol to the precipitate, stir, let stand for refrigerated (temperature 2-10°C) 10°C) for 10 hours, and the supernatant was collected and filtered.

[0024] (3) Combine the filtrates, recover ethanol and concentrate to a clear paste with a relative density of 1.35 at 70°C, add 5 times the amount of water-in-oil (W / O) emulsion base containing 6% borneol, and prepare an external ointment. For example: put glyceryl monostearate, paraffin, white petrolatum, liquid paraffin, and Span-80 in a container, heat and melt on a water bath, keep th...

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Abstract

The invention discloses external sarcandra glabra ointment and a preparation method thereof. The external sarcandra glabra ointment is prepared from sarcandra glabra by the processes of water extraction, ethanol precipitation, filtration, concentration and the like. The external ointment has an obvious anti-inflammatory and analgesic effects, is easy to prepare, and has remarkable and economical and social benefits.

Description

technical field [0001] The invention belongs to the technical field of preparation of Chinese herbal medicines, and in particular relates to a sarcophagus ointment for external use and a preparation method thereof. Background technique [0002] Zhongjiefeng (or Jiujiecha) is a traditional Chinese medicinal material recorded in the "Chinese Pharmacopoeia". It is commonly used in folk herbs in southern and southwestern provinces of my country. Sarcandra glabra (Thunb.) Nakai The dry whole grass (or above-ground parts). [0003] Sarcophagus has been widely used in anti-inflammatory and analgesic drugs, lozenges for lozenges, blood-heat purpura medicine, and there are tablets, capsules, injections, and oral liquids of single medicines, such as Sargassum Tablets, Qingrexiaoyanning Capsules, Zhongjiefeng Injection, Xuekang Oral Liquid, etc. However, according to the Chinese Pharmacopoeia and drug standards issued by the Ministry, there is no medicine for external use of Jiujiech...

Claims

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Application Information

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IPC IPC(8): A61K36/185A61K9/06A61P29/00
Inventor 陈强陈达鑫李杰
Owner FUJIAN UNIV OF TRADITIONAL CHINESE MEDICINE
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