Method for extracting taurine from mussel
A technology of taurine and mussels, applied in chemical instruments and methods, preparation of organic compounds, organic chemistry, etc., can solve the problems of high extraction cost and low purity of taurine, and achieve low extraction cost and simple and effective method , high extraction rate and high purity
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Embodiment 1
[0027] (1) Homogenization: Weigh 2Kg of washed mussel meat, mash it into a slurry, add distilled water, and stir evenly to obtain a homogenate, wherein the mass ratio of mussel meat to distilled water is 1:3.
[0028] (2) Ultrasonic crushing: The homogenate was treated with an ultrasonic wave with a power of 420W for 50 minutes at a constant temperature of 45°C to obtain a crushing liquid.
[0029] (3) Extraction: heat and boil the crushed liquid in a boiling water bath for 1.5 hours, filter the crushed liquid with gauze to obtain the extract and filter residue, repeat the extraction of the filter residue twice according to steps (1)~(3), and combine the extract.
[0030] (4) Secondary separation: add 10% sulfosalicylic acid to the extract, the mass ratio of sulfosalicylic acid to extract is 1:5, centrifuge the extract to obtain the supernatant The supernatant was ultrafiltered under a pressure of 1.5MPa with an ultrafiltration membrane with a molecular cut-off of 1000Da to ob...
Embodiment 2
[0035] (1) Homogenization: Weigh 2Kg of washed mussel meat, mash it into a slurry, add distilled water, and stir evenly to obtain a homogenate, wherein the mass ratio of mussel meat to distilled water is 1:4.
[0036] (2) Ultrasonic crushing: The homogenate was treated with an ultrasonic wave with a power of 400W for 60 minutes at a constant temperature of 40°C to obtain a crushing liquid.
[0037] (3) Extraction: heat and boil the crushed liquid in a boiling water bath for 2 hours, filter the crushed liquid with gauze to obtain the extract and filter residue, repeat the extraction of the filter residue twice according to steps (1)~(3), and combine the extract.
[0038](4) Secondary separation: add 10% sulfosalicylic acid to the extract, the mass ratio of sulfosalicylic acid to extract is 1:7, centrifuge the extract to obtain the supernatant The supernatant was ultrafiltered under a pressure of 1.7MPa with an ultrafiltration membrane with a molecular cut-off of 1000Da to obtai...
Embodiment 3
[0043] (1) Homogenization: Weigh 2Kg of washed mussel meat, mash it into a slurry, add distilled water, and stir evenly to obtain a homogenate, wherein the mass ratio of mussel meat to distilled water is 1:6.
[0044] (2) Ultrasonic crushing: The homogenate was treated with an ultrasonic wave with a power of 450W for 30 minutes at a constant temperature of 50°C to obtain a crushing liquid.
[0045] (3) Extraction: Heat and boil the crushed solution in a boiling water bath for 1 hour, filter the crushed solution with gauze to obtain the extract and filter residue, repeat the extraction of the filter residue twice according to steps (1)~(3), and combine the extract.
[0046] (4) Secondary separation: add 10% sulfosalicylic acid to the extract, the mass ratio of sulfosalicylic acid to extract is 1: 10, centrifuge the extract to obtain the supernatant The supernatant was ultrafiltered under a pressure of 2 MPa with an ultrafiltration membrane with a molecular cut-off of 1000 Da to...
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