Method for preparation of graphite surface silicon carbide coating
A silicon carbide coating and graphite technology, applied in the field of silicon carbide coating on graphite surface, can solve the problems of high energy consumption, complex production process, low performance of graphite silicon carbide material, etc., and achieve the effects of reduced energy consumption and simple process
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Embodiment 1
[0022] A method for silicon carbide coating on a graphite surface, comprising:
[0023] Take 99.99% of the graphite material and silane and mix them in a weight ratio of 1:1 to make a graphite silane mixed material, then pretreat according to the furnace, turn on the electricity to heat up, secondly heat up and keep warm, three times heat up and keep warm, four times heat up, keep warm and The temperature is lowered; the furnace pretreatment is filled with nitrogen, nitrogen is filled during the electrification and heating process, and nitrogen and hydrogen gas are filled during the four heating and heat preservation processes. The details are as follows:
[0024] Furnace pretreatment: evacuate the deposition furnace to -10KPa and let it stand for 1.5 minutes, then fill the deposition furnace with nitrogen until the furnace reaches the normal pressure position;
[0025] Power on and heat up: After the pretreatment of the deposition furnace, put the graphite-silane mixed materi...
Embodiment 2
[0031] A method for silicon carbide coating on a graphite surface, comprising:
[0032] Take 99.99% graphite material and silane and mix them in a weight ratio of 1 to 1 to make a graphite silane mixed material, then pretreat according to the furnace, power on and heat up, heat up twice, keep warm, heat up three times, keep warm, heat up four times, keep warm and The temperature is lowered; the furnace pretreatment is filled with nitrogen, nitrogen is filled during the electrification and heating process, and nitrogen and hydrogen gas are filled during the four heating and heat preservation processes. The details are as follows:
[0033] Furnace pretreatment: evacuate the deposition furnace to -10KPa and let it stand for 2 minutes, then fill the furnace with nitrogen until the furnace reaches normal pressure;
[0034] Power on and heat up: After pretreatment of the deposition furnace, put the graphite-silane mixed material into the furnace, turn on the power switch of the depo...
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