Preparation method of chemically modified asphalt
A chemical modification and asphalt technology, applied in the field of chemically modified asphalt preparation, can solve the problems of useless improvement of molecular structure, precipitation and separation, poor flexibility, etc. relay effect
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Embodiment 1
[0017] A method for preparing chemically modified asphalt: under the action of an initiator, the method reacts base asphalt with naphthalene vinyl compounds to prepare chemically modified asphalt. The steps are as follows:
[0018] 1) Add 100 parts of petroleum pitch heated to 90~130 ℃ (mass, the same below) into the reactor, and add 0.3 parts of initiator benzoyl peroxide;
[0019] 2) Raise the temperature to 130 °C, add 1.5 parts of butadiene and 5 parts of 2-vinylnaphthalene, and pass N 2 Keep the pressure of the reactor at 0.2 MPa, react for 4 h, and then degas for 20 min. After filtration, the modified asphalt with greatly improved low-temperature toughness is obtained.
Embodiment 2
[0021] Yet another method for preparing chemically modified asphalt: under the action of an initiator, the base asphalt is reacted with allyl sulfide compounds to obtain chemically modified asphalt. In this method, allyl sulfide The compound replaces the naphthalene vinyl compound, and the steps are as follows:
[0022] 1) Add 100 parts of petroleum pitch heated to 90~130 ℃ (mass, the same below) into the reactor, and add 0.8 parts of initiator benzoyl peroxide;
[0023] 2) Raise the temperature to 120 °C, add 5 parts of diallyl sulfide and 1.2 parts of isoprene, maintain the pressure at 0.3 MPa, react for 5 h, degas and filter, and then obtain modified asphalt with greatly improved low-temperature toughness.
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