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43results about How to "Prevent oxidative denaturation" patented technology

System for measuring wettability of high-temperature and high-chemical-activity liquid metal lithium

The invention discloses a system for measuring the wettability of high-temperature and high-chemical-activity liquid metal lithium. The system comprises a vacuum chamber, a vacuum air-extraction and measurement system, a sample table, a heating system, a sample driving system, a liquid lithium dropping-in system, a light source, a camera and an image processing system. The oxidization denaturation of the surface of the liquid lithium is stopped in a high-vacuum environment; the liquid lithium dropping-in system with ingenious design implements dropping-in of the liquid lithium; a heating wire and a temperature measurement system are arranged on the sample table in a sheathed manner, so that a requirement on the measurement of the wettability of the high-temperature liquid lithium is met; a contact angle of the liquid lithium on a substrate is measured by an image analysis method and through a programmed Matlab batch processing program. The system provided by the invention can be used for quickly, economically and effectively testing the wettability of the high-temperature and high-chemical-activity liquid metal lithium to the surface of the substrate and supplies excellent experiment and data accumulation to possible application of a first wall of the liquid lithium to a future fusion reactor.
Owner:INST OF PLASMA PHYSICS CHINESE ACAD OF SCI

Modified-graphene-containing tungsten carbide spraying powder used for preparing self-lubricating abrasion-resistant coating

The invention provides modified-graphene-containing tungsten carbide spraying powder used for preparing a self-lubricating abrasion-resistant coating. A method comprises the following steps that (1) a certain amount of a modified graphene / nano tungsten carbide composite is weighed and mixed with a certain amount of absolute ethyl alcohol, and a mixed solution of a graphene / nano tungsten carbide composite is obtained after ultrasonic dispersion; (2) a certain amount of tungsten carbide / cobalt spraying powder is weighed and added into the mixed solution of the graphene nano tungsten carbide composite; (3) modified graphene composited tungsten carbide / cobalt spraying powder is obtained through a vacuum freeze drying method; and (4) the modified graphene composited tungsten carbide / cobalt self-lubricating abrasion-resistant coating is prepared on the surface of a part subjected to cleaning and sand blasting through a thermal spraying process. According to the modified-graphene-containing tungsten carbide spraying powder, the layered single-layer carbon structure characteristics of graphene are reserved, the proportion of the graphene is increased through grown nano carbide particles, and in addition, losses of the graphene caused by ball milling or other powder mixing processes can be avoided through the freeze drying method.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Drying device for edible/medical/feed insects

The invention discloses a drying device for edible / medical / feed insects. A carbon dioxide gas inlet pipe is arranged on the side wall of a heat preservation drying box body, one end of the carbon dioxide gas inlet pipe extends into the bottom of the heat preservation drying box body, and the other end of the carbon dioxide gas inlet pipe extends out of the box body to be connected with a carbon dioxide gas inlet valve. The top end of the heat preservation drying box body is provided with an exhaust opening, and the bottom end of the heat preservation drying box body is provided with a gas inlet. The exhaust opening is connected with a hot air outlet pipe which is provided with a one-way air pressurizing valve, and the position, between the one-way air pressurizing valve and the exhaust opening, on the hot air outlet pipe is further provided with a carbon dioxide gas outlet valve. The other end of the hot air outlet pipe is connected with a silica gel drier, a filter, an air heater and a hot air inlet pipe in sequence. The hot air inlet pipe is connected with the gas inlet, and the one-way air pressurizing valve is installed on the hot air inlet pipe. A plurality of layers of trays are arranged in the heat preservation drying box body, and the bottoms of the trays are in screen shape. A movable door is further arranged on the heat preservation drying box body, a temperature controller is arranged in the heat preservation drying box body, and the temperature controller is electrically connected with the air heater.
Owner:INST OF ZOOLOGY GUANGDONG ACAD OF SCI

Preparation method for graphene modified thermal spraying powder of heat-indicating thermal barrier coating

The invention provides a preparation method for modified-graphene-containing tungsten carbide spraying powder of a self-lubricating and wear-resisting coating. The preparation method comprises steps as follows: 1), a certain quantity of modified graphite/tungsten carbide nano-composites are weighed and mixed with a certain amount of absolute ethyl alcohol, and after ultrasonic dispersion, a mixed solution of a graphite/tungsten carbide nano-composite is obtained; 2), a certain amount of tungsten carbide/cobalt spraying powder is weighed and added to the mixed solution of the graphite/tungsten carbide nano-composite; 3), tungsten carbide/cobalt spraying powder composited with modified graphene is obtained with a vacuum freeze drying method; 4), a tungsten carbide/cobalt self-lubricating and wear-resisting coating composited with modified graphene is prepared with a thermal spraying technology on the surface of a part after cleaning and sand blasting. According to the preparation method, characteristics of a laminated single-layer carbonaceous structure of graphene are reserved, a ratio of graphene is further increased by growing carbide nano-particles, and besides, with the adoption of the freeze drying method, loss of graphene due to ball milling or other powder mixing technologies can be avoided.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Piperidine type ionic liquid and preparation method and application thereof

ActiveCN109627227AGood and stable electrochemical performanceLower impedanceSulfonic acid amide preparationEvaporationElectrochemical window
The invention discloses a method for preparing piperidine type ionic liquid. The preparation method comprises the following steps of adding bromopropane into ethyl acetate, then adding N-methyl piperidine for a reaction for 8-48 h, eluting a solid phase with acetone, and performing rotary evaporation to obtain an intermediate product; dissolving the intermediate product in water, adding lithium trifluoromethanesulfonimide, washing an organic phase with water after extraction and liquid separation, and conducting rotary steaming and drying to obtain a final product. Meanwhile, the invention also discloses the piperidine type ionic liquid prepared by the method and application of the piperidine type ionic liquid as an electrolyte component of a lithium ion battery. The preparation method isimplemented at the normal temperature and has the advantages of being high in yield, economical and simple in operation. The piperidine type ionic liquid has the advantages of high purity, low water content, low viscosity, high conductivity and wide electrochemical window. The piperidine type ionic liquid prepared by the method is used as the electrolyte component to be applied to an electrolyte of the lithium ion battery and shows better inflammability and chemical stability and lower electrochemical impedance.
Owner:ZHEJIANG UNIV OF TECH

Preparation process of high content conjugated unsaturated trienic acid granada seed oil

InactiveCN100510041CGive full play to the high extraction efficiencyHigh yieldFatty-oils/fats productionPOMEGRANATE SEED OILPurification methods
The invention belongs to the field of extraction and separation technology of plant active ingredients, and relates to a preparation method for extracting high-content conjugated unsaturated trienoic acid pomegranate seed oil from plant seeds. The preparation method of a high-content conjugated unsaturated trienoic acid pomegranate seed oil of the present invention is to extract, separate and purify the conjugated unsaturated trienoic acid from pomegranate seeds, and is divided into the following steps: pulverizing the pomegranate seeds Finally, it is loaded into an extraction kettle for carbon dioxide extraction; the extracted carbon dioxide fluid is passed through a rectification column, and the supercritical rectification method is used to purify and remove impurities and other saturated fatty acids and monounsaturated fatty acids to obtain high-content conjugated unsaturated fatty acids. Saturated trienoic acid oil; then pass through a separation tank to separate other impurities and carbon dioxide. This method is a new process technology combining supercritical or subcritical extraction and rectification, which can prevent the oxidative denaturation of conjugated unsaturated trienoic acid, keep the product from being polluted, and obtain a high content of conjugated unsaturated trienoic acid. Saturated trienoic acid oil.
Owner:GUANGZHOU HONSEA SUNSHINE BIOTECH CO LTD

Special compound premix feed for producing selenium-enriched pork and production method of special compound premix feed

The invention relates to a special compound premix feed for producing selenium-enriched pork and a production method of the special compound premix feed. 1 weight percent of the premix feed is added into a raw feed, the premix feed is suitable for 120-day-age growing-finishing pigs to pig in slaughter stage, the content of selenium of the produced pork is 0.25-0.29mg/kg, the requirements of the pigs on selenium can be met, and the healthy growth of the pigs is guaranteed. A used selenium source is nano-selenium or selenium yeast, the nano-selenium is nano-scale elemental selenium by taking macromolecular substances such as proteins and saccharides as dispersing agents and has the characteristics of small particle size, large superficial area, instability and the like, the selenium yeast is a high-quality organic selenium source, the nano-selenium or selenium yeast is more easily absorbed by the organism compared with other selenium sources such as sodium selenite and amino acid chelated selenium, and has the relatively high bioavailability, safety and oxidation resistance, the selenium-enriched pork belongs to functional healthy pork with a selenium supplement effect, the selenium contained in the selenium-enriched pork is the organic selenium which is easily absorbed and utilized by the human body, and the selenium-enriched pork is an excellent selenium supplement food.
Owner:福建光华农牧科技开发有限公司

A high-temperature, highly chemically active liquid metal lithium wettability measurement system

The invention discloses a system for measuring the wettability of high-temperature and high-chemical-activity liquid metal lithium. The system comprises a vacuum chamber, a vacuum air-extraction and measurement system, a sample table, a heating system, a sample driving system, a liquid lithium dropping-in system, a light source, a camera and an image processing system. The oxidization denaturation of the surface of the liquid lithium is stopped in a high-vacuum environment; the liquid lithium dropping-in system with ingenious design implements dropping-in of the liquid lithium; a heating wire and a temperature measurement system are arranged on the sample table in a sheathed manner, so that a requirement on the measurement of the wettability of the high-temperature liquid lithium is met; a contact angle of the liquid lithium on a substrate is measured by an image analysis method and through a programmed Matlab batch processing program. The system provided by the invention can be used for quickly, economically and effectively testing the wettability of the high-temperature and high-chemical-activity liquid metal lithium to the surface of the substrate and supplies excellent experiment and data accumulation to possible application of a first wall of the liquid lithium to a future fusion reactor.
Owner:INST OF PLASMA PHYSICS CHINESE ACAD OF SCI

A kind of piperidine type ionic liquid and its preparation method and application

The invention discloses a method for preparing piperidine type ionic liquid. The preparation method comprises the following steps of adding bromopropane into ethyl acetate, then adding N-methyl piperidine for a reaction for 8-48 h, eluting a solid phase with acetone, and performing rotary evaporation to obtain an intermediate product; dissolving the intermediate product in water, adding lithium trifluoromethanesulfonimide, washing an organic phase with water after extraction and liquid separation, and conducting rotary steaming and drying to obtain a final product. Meanwhile, the invention also discloses the piperidine type ionic liquid prepared by the method and application of the piperidine type ionic liquid as an electrolyte component of a lithium ion battery. The preparation method isimplemented at the normal temperature and has the advantages of being high in yield, economical and simple in operation. The piperidine type ionic liquid has the advantages of high purity, low water content, low viscosity, high conductivity and wide electrochemical window. The piperidine type ionic liquid prepared by the method is used as the electrolyte component to be applied to an electrolyte of the lithium ion battery and shows better inflammability and chemical stability and lower electrochemical impedance.
Owner:ZHEJIANG UNIV OF TECH

Preparation method of freeze-dried liposome containing hair-growing composition

The invention relates to a preparation method of a freeze-dried liposome containing a hair-growing composition. The preparation method is characterized by comprising the following steps: A, weighing amentoflavone, quercetin-3-o rutinoside, tetramethylpyrazine and ricinoleic acid according to a mass ratio of 1: (1-3): (0.5-2): (3-5) to form the hair-growing composition, and weighing hyaluronic acidoligosaccharide and scleroglucan according to a mass ratio of 1: (0.2-0.5) to form a freeze-drying protective agent; B, dissolving the hair-growing composition, cholesterol and hydrogenated lecithinin ethanol, performing ultrasonic treatment, and performing reduced-pressure rotary evaporation to remove ethanol to obtain a lipid membrane containing the hair-growing composition; C, adding an isotonic phosphate buffer solution into the lipid membrane, and performing ultrasonic treatment and filtration to obtain a liposome suspension; and D, adding the freeze-drying protective agent into the liposome suspension, and performing vacuum freezing at the temperature of minus 50 DEG C to minus 10 DEG C for 36-72 hours to obtain the freeze-dried liposome containing the hair-growing composition. Thefreeze-dried liposome containing the hair-growing composition has the advantages of uniform particle size, high stability, convenience in use and good hair-growing effect.
Owner:PROYA COSMETICS

Method for extracting hydroxytyrosol from olive fruits

The invention discloses a method for extracting hydroxytyrosol from olive fruits, which comprises the steps of weighing a proper amount of olive fruit powder, adding a sulfuric acid aqueous solution for acid hydrolysis extraction, and keeping the temperature at 80-90 DEG C; adjusting the pH value of the extracted extracting solution to 5-7 by using a NaOH solution to obtain a slightly neutral extracting solution; extracting the slightly neutral extracting solution with ethyl acetate, wherein the volume ratio of the slightly neutral extracting solution to the ethyl acetate is 1: (3-5), and a hydroxytyrosol extracting solution is obtained; and carrying out concentration and crystallization on the hydroxytyrosol extraction liquid, then conducting vacuum freeze drying, and obtaining a hydroxytyrosol finished product with the content of 45%-50%, wherein the mass of the obtained hydroxytyrosol finished product is 0.3%-0.8% of the mass of the olive fruit powder. The acid hydrolysis method is adopted for extraction, compared with an enzyme method, the production cost is low, the method is simple, convenient and easy to operate, the sulfuric acid solution is used for hydrolysis, the stability of the property of the plant extract can be kept, and oxidative denaturation of hydroxytyrosol is prevented; bacterial pollution in the extraction process is prevented; and the yield of hydroxytyrosol obtained by hydrolyzing oleuropein in the fruits can be improved.
Owner:陕西富恒生物科技有限公司 +1
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