The invention provides a method for preparing pleonaste from
zinc hydrometallurgy iron
slag, which comprises the following steps: carrying out first acid leaching on the
zinc hydrometallurgy iron
slag, then adjusting the pH value, and carrying out
solid-liquid separation to obtain first leaching
slag; the first leaching residues and a
magnesium source are mixed and roasted, and roasted clinker is obtained; the
roasting clinker is subjected to second acid leaching,
solid-liquid separation is conducted, and second leaching residues are obtained; and the second leaching residues are subjected to
magnetic separation, and pleonaste is obtained. According to the method,
zinc and
calcium elements in the zinc
hydrometallurgy iron slag are directionally separated through step-by-step leaching and
roasting, the iron element is separated and converted into pleonaste with high
magnetism and stability, the requirements of high-value fields such as
refractory materials are met, and effective separation of the elements and high-value utilization of the zinc hydrometallurgy iron slag are achieved.