New compound and extraction method and application thereof
An extraction method and compound technology, applied in steroids, medical preparations containing active ingredients, organic chemistry, etc., can solve problems such as insufficient research
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Embodiment 1
[0120] Example 1 : Extraction of the compound of the present invention
[0121] A. Pretreatment of Pandanus raw materials
[0122] The pandanus raw medicinal material was dried at a temperature of 70°C for 0.8 hours, and the water content of the pandanus raw medicinal material was 0.45%, and then the dried pandanus was crushed to -60 mesh crushed to obtain Pandanus powder;
[0123] B. Extraction
[0124] In the pilot test multi-functional extraction tank produced by Hunan Hengyang Pharmaceutical Equipment Factory, the pandanus powder obtained in step A) is heated in steam with 90% ethanol aqueous solution according to the weight ratio of the pandanus powder to the ethanol aqueous solution of 1.0:10 Extract under reflux for 1.0 hour, after filtration, repeat the extraction of the residue 3 times, combine all the obtained extracts, concentrate under reduced pressure, and dry to obtain a dry extract;
[0125] C. Extraction
[0126] Add water to the dry extract according to ...
Embodiment 2
[0144] Example 2 : Extraction of the compound of the present invention
[0145] Proceed in the same manner as in Example 1, except that 85% aqueous ethanol is used for extraction, and dichloromethane is used as the extractant at a temperature of 90°C. Other conditions are the same as in Example 1, and the product of the present invention is also obtained.
Embodiment 3
[0146] Example 3 : Extraction of the compound of the present invention
[0147] Proceed in the same manner as in Example 1, except that 95% aqueous ethanol is used for extraction, and ethyl acetate is used as the extractant at a temperature of 75°C. Other conditions are the same as in Example 1, and the product of the present invention is also obtained.
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