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Device and method for spinning nanofiber and filament composite yarns

A nanofiber, filament technology, applied in the direction of filament/thread forming, fiber processing, yarn, etc., can solve problems such as easy peeling, and achieve the effect of high strength characteristics

Active Publication Date: 2015-02-11
JIANGNAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Nanofibers are easy to adhere to the filaments due to their good adhesion properties and surface adsorption, but they are also easy to peel off

Method used

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  • Device and method for spinning nanofiber and filament composite yarns

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Embodiment one: the spinning method of nanofiber and long filament composite yarn, adopts following process step:

[0029] (1) Acetone: dimethylacetamide is formulated into a uniform spinning solvent at a volume ratio of 2:1, and cellulose diacetate with a molecular weight distribution of 30,000 and acetylation of 39.8% is dissolved in the spinning solvent, Stirring at room temperature at 25°C for 12 hours to obtain a uniform spinning solution, the mass fraction of cellulose diacetate in the spinning solution was 11%;

[0030] (2) Add the spinning solution to two spinning solution syringes for electrospinning, the distance between the two spinning solution injectors is 15cm, and the distance between the yarn guide and the nanofiber receiving tray is 15cm; spinning The liquid injector is connected to the positive pole of the high-voltage power supply, and the nanofiber receiving plate is connected to the negative pole of the high-voltage power supply; the voltage of the ...

Embodiment 2

[0033] Embodiment two: the spinning method of nanofiber and long filament composite yarn, adopt following process step:

[0034] (1) Dissolve polyacrylonitrile with a relative molecular weight of 75,000 in dimethylacetamide, and stir at room temperature at 28°C for 12 hours to obtain a uniform spinning solution. The mass fraction of polyacrylonitrile in the spinning solution is 10%;

[0035](2) Add the spinning solution into two spinning solution syringes respectively, the distance between the two spinning solution injectors is 10cm, and the distance between the yarn guide and the receiving tray is 10cm; the spinning solution injector is connected to the positive pole of the high voltage power supply , the nanofiber receiving plate is connected to the negative pole of the high-voltage power supply, the electrospinning voltage is 30kV, the spinning speed is 0.5ml / hour, the spinning ambient temperature is 28°C, and the relative humidity of the spinning environment is 50%RH. The ...

Embodiment 3

[0038] Embodiment three: the spinning method of composite yarn of nanofiber and long filament, adopt following process steps:

[0039] (1) Dissolve polylactic acid with an average molecular weight of 10,000 in dichloromethane, and stir at room temperature of 25°C for 12 hours to obtain a uniform spinning solution. The mass fraction of polylactic acid in the solution is 8%;

[0040] (2) Add the spinning solution to two spinning solution injectors respectively, the distance between the two spinning solution injectors is 8cm, the distance between the yarn guide and the nanofiber receiving tray is 8cm; the spinning solution injector is connected to high pressure The positive pole of the power supply, the nanofiber receiving tray is connected to the negative pole of the high-voltage power supply, the electrospinning voltage is 15kV, the spinning speed is 0.8ml / hour, the spinning ambient temperature is 25°C, and the relative humidity of the spinning environment is 60%RH. The nanofibe...

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Abstract

The invention relates to a device for spinning a nanofiber and filament composite yarn; the device is characterized by comprising a left side spinning solution injector and a right side spinning solution injector, wherein the left side spinning solution injector and the right side spinning solution injector are connected with a high voltage power supply anode; receiving plates are connected with a high voltage power supply cathode; a left side filament leading-in device and a right side filament leading-in device are arranged on external sides of a left side receiving plate and a right side receiving plate; and winding devices are arranged below the left side receiving plate and the right side receiving plate. The device for spinning the nanofiber and filament composite yarn, provided by the invention, has the following technical steps of: (1) carrying out electrostatic spinning; (2) leading in filaments to the two nanofiber receiving plates during electrostatic spinning, so that the nanofibers adhere to the two filaments; and (3) twisting and combining the two filaments, so as to obtain the nanofiber and filament composite yarn. According to the invention, the obtained nanofiber and filament composite yarn has the advantages of ultrahigh specific surface area of the nanofiber and high-strength characteristic of the filament.

Description

technical field [0001] The invention relates to a composite yarn spinning method, in particular to a spinning device and a spinning method for a nanofiber and filament composite yarn, belonging to the technical field of composite yarn production. Background technique [0002] Electrospinning technology is an effective method to prepare nanofibers and fiber membranes, but the extremely low strength of nanofibers and nanofiber membranes is an important obstacle to their further application in industrial related fields. The tenacity of filaments, especially nylon-based filaments, is one of the most sought-after characteristics for industrial applications. If the nano effect of electrospun nanofibers and the strength of filaments can be effectively combined to produce a new type of nano / filament composite yarn, it will open up a new field of industrial application of nanofibers. [0003] Electrospinning technology is a spinning technology that produces nanoscale fibers by apply...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D02G3/22D01D5/00
Inventor 杨瑞华杨广磊高卫东王鸿博
Owner JIANGNAN UNIV