Unidirectional transparent composite magnet and preparation method
A composite magnet, transparent technology, applied in the direction of inductor/transformer/magnet manufacturing, permanent magnet, inorganic material magnetism, etc., can solve the problem of limiting functional magnetic materials, and achieve the effect of simple process and cost reduction
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[0026] The invention relates to a one-way transparent composite magnet and a preparation method thereof. The preparation method of a kind of unidirectional transparent composite magnet provided by the present invention comprises the following steps:
[0027] Step 1) preparation of particle composite system
[0028] Add 5 to 100 parts of ferromagnetic particles with an average size of 0.1 to 100 μm into 100 parts of thermosetting or thermoplastic organic monomers, stir and disperse at 20 to 250 °C for 0.5 to 10 hours; After uniform dispersion, add 1-15 parts of curing agent or cross-linking agent, and continue stirring for 30 seconds.
[0029] Step 2) Orientation of Magnetic Particles in Magnetic Field
[0030] The dispersion composite system is injected into the mould, and then a magnetic field is applied at the mould, the magnetic field strength is 0.01-2.0T, and the orientation time is 1-60min.
[0031] Step 3) Curing
[0032] Place the oriented and formed sample in an o...
Embodiment 1
[0036] Add 10 parts of Fe powder with an average particle size of 0.1 μm to 100 parts of unsaturated polyester monomer, stir and disperse in a water bath at 20°C for 5 hours; after the system is uniformly dispersed, add 5 parts of crosslinking agent styrene, Continue stirring for 30s.
[0037] The dispersion composite system is injected into the mold, and then a magnetic field is applied at the mold, the magnetic field is generated by an electromagnetic coil, the magnetic field strength is 0.1T, and the orientation time is 5min.
[0038] Put the oriented sample into an oven for curing, the temperature of the oven is 20°C, and the temperature is kept for 480h.
[0039] The prepared sample has dense structure, low porosity and smooth surface. Metallographic observation was carried out on the sample prepared in Example 1, and it was found that Fe in the polymer matrix was distributed in chain-like clusters along the direction of the external magnetic field. The saturation magne...
Embodiment 2
[0041] Add 5 parts of Co powder with an average particle size of 1.5 μm to 100 parts of epoxy resin monomer, stir and disperse in a water bath at 60 ° C for 0.5 h; after the system is uniformly dispersed, add 15 parts of curing agent polyamide, continue Stir for 30s.
[0042] The dispersion composite system is injected into the mold, and then a magnetic field is applied at the mold. The magnetic field is generated by an electromagnet, the magnetic field strength is 0.8T, and the orientation time is 10 minutes.
[0043] Put the oriented sample into an oven for curing, the temperature of the oven is 80°C, and keep it warm for 20h.
[0044] The prepared sample has dense structure, low porosity and smooth surface. Metallographic observation was carried out on the sample prepared in Example 2, and it was found that Co in the polymer matrix was distributed in chain-like clusters along the direction of the external magnetic field. The saturation magnetization of the sample tested b...
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