Black film, substrate with black film, and image display device, and black resin composition and black material dispersion
A technology of black resin and black film, applied in the field of black film, can solve the problems of complicated manufacturing process of black matrix and reduced bonding between black matrix and substrate, etc.
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Embodiment
[0360] Hereinafter, although an Example demonstrates this invention concretely, this invention is not limited to these Examples at all.
[0361]
[0362] (Each measurement, evaluation method)
[0363] Each measurement or evaluation method used in Examples or Comparative Examples, such as properties of materials and sheets, is shown below.
[0364] Content rate of silver component in black material
[0365] The content of the silver component in the black material (silver-tin alloy particles or the mixed particles of silver-tin alloy particles and silver particles) is obtained by the following method: using an electron beam microanalyzer (EPMA: JXA8800, manufactured by JEOL Ltd.) The powder compact of the black material powder was analyzed, and qualitative analysis and quantitative analysis were performed using a wavelength dispersive X-ray spectrometer, thereby measuring the content ratio (mass ratio) of tin and silver in the powder.
[0366] Average dispersed particle dia...
Embodiment A1
[0376] Production of black film
[0377] Silver tin colloidal liquid (mixed particle dispersion liquid of silver tin alloy particles and silver particles, manufactured by Sumitomo Osaka Cement Co., Ltd., solid content: 30% by mass, average dispersed particle diameter: 10nm, particle size distribution index D90%: 40nm, silver component Content: 91% by mass, type of dispersant: polyurethane-based random copolymer, amount of dispersant added: 15 parts by mass), resist (dispersion medium: PGMEA, solid content : 1% by mass) so that the solid content volume ratio (silver tin colloid: resist) was 3:97, and dispersed by ultrasonic treatment to form a black paint. In addition, the above-mentioned solid content volume ratio is a charging ratio.
[0378] Next, the particle size distribution of the black paint was measured by the method described above. As a result, the average dispersed particle diameter was 13 nm, and the particle size distribution index D90% was 48 nm.
[0379] Then,...
Embodiment A2
[0385] Except having added the resist so that solid content volume ratio may become 7:93 in preparation of the black film of Example A1, the base material with a black film was produced similarly to Example A1, and it evaluated similarly.
[0386] The results are summarized in Table 1.
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