tizrnb hip joint prosthesis and preparation method thereof
A hip joint prosthesis, alloy matrix technology, applied in the direction of prosthesis, medical science, coating, etc., can solve the problem of insufficient bonding strength of hydroxyapatite or β-TCP coating and titanium coating, hydroxyapatite or β-TCP coating peeling off and other problems
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Embodiment 1
[0018] The Ti13Nb13Zr alloy joint shank with an elastic modulus of 65GPa was sandblasted with alumina with a particle size of 50 mesh for 4 minutes to make the surface rough and remove the surface layer. Then put it into the plasma vacuum chamber, evacuate to 0.133Pa, and then fill it with Ar. The spray gun is 300mm away from the joint handle, and the plasma preheats the joint handle for 4 minutes to about 400°C, and the plasma sputtering cleans for 4 minutes. The 300-mesh Ti13Nb13Zr powder is fed by the powder feeder and sprayed to a 25μm dense layer at a voltage of 60V and 600A. The outer layer is sprayed with β-TCP powder of 60 meshes, sprayed at 60V and 600A with a thickness of 50 μm and an average pore size of 150 μm.
[0019] After cooling, the Ti13Nb13Zr alloy joint handle sprayed with bioactive composite coating was taken out. According to ISO13779-4, the bond strength of β-TCP coating is 35MPa.
Embodiment 2
[0021] The Ti13Nb13Zr alloy joint shank with an elastic modulus of 65GPa was sandblasted with alumina with a particle size of 50 mesh for 4 minutes to make the surface rough and remove the surface layer. Then put it into the plasma vacuum chamber, evacuate to 0.133Pa, and then fill it with Ar. The spray gun is 300mm away from the joint handle, the plasma preheats the joint handle for 4 minutes, reaches about 400°C, and the plasma sputtering is cleaned for 4 minutes, and the powder feeder feeds 300 mesh Ti13Nb13Zr powder and sprays it to a 25μm dense layer at a voltage of 60V and 600A , and then sprayed with 150 mesh Ti13Nb13Zr powder at 60V and 600A to a porous layer with a thickness of 50 μm and an average pore diameter of 150 μm. The outer layer is sprayed with β-TCP powder of 60 meshes, sprayed at 60V and 600A with a thickness of 50 μm and an average pore size of 150 μm.
[0022] After cooling, the Ti13Nb13Zr alloy joint handle sprayed with bioactive composite coating was ...
Embodiment 3
[0024] The Ti13Nb13Zr alloy joint shank with an elastic modulus of 65GPa was sandblasted with alumina with a particle size of 50 mesh for 4 minutes to make the surface rough and remove the surface layer. Then put it into the plasma vacuum chamber, evacuate to 0.133Pa, and then fill it with Ar. The spray gun is 300mm away from the joint handle, the plasma preheats the joint handle for 4 minutes, reaches about 400°C, and the plasma sputtering is cleaned for 4 minutes, and the powder feeder feeds 300 mesh Ti13Nb13Zr powder and sprays it to a 25μm dense layer at a voltage of 60V and 600A , and then spray 60-mesh tantalum powder to a porous layer with a thickness of 100 μm and an average pore diameter of 200 μm at 60V and 600A. 60-mesh β-TCP powder is used for spraying β-TCP on the outer layer. The spraying thickness is 50 μm under 60V and 600A, and the average pore size is 150 μm.
[0025] After cooling, the Ti13Nb13Zr alloy joint handle sprayed with bioactive composite coating w...
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