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Compound annular electrode electrostatic spinning device

A ring-shaped electrode, electrospinning technology, applied in textiles and papermaking, filament/thread forming, fiber processing, etc. Effective protection of the solution, etc., to reduce high-voltage damage to the instrument or cause harm to the human body, avoid direct contact, and have a reliable principle.

Inactive Publication Date: 2013-07-24
QINGDAO UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, one of the main means of preparing continuous one-dimensional micro-nano fibers is electrospinning technology, which has good development prospects in the fields of filter materials, sound-absorbing and sound-absorbing materials, special protective clothing, electronic sensors, and textile engineering. Micro-nano fibers prepared by electrospinning have many characteristics such as large specific surface area and high porosity that are not possessed by fibers prepared by traditional stretching methods and melt-blown methods. Low, unable to meet the needs of industrialization
The main means to increase the spinning yield in the prior art is the improved design of the spinning method, such as the array multi-nozzle electrospinning equipment disclosed in Chinese patent 200910031948.2 and the coaxial composite continuous micro / nano fiber multi-nozzle disclosed in Chinese patent 200310109222.9 Electrospinning devices improve spinning efficiency by increasing the number of spinneret heads; the bubble electrospinning device disclosed in Chinese patent 201210177134.1 utilizes explosive bubbles to generate multiple jets to achieve rapid preparation of electrospinning; Czech ELMARCO company The first generation of "nano spider" series equipment produced adopts cylindrical rotating electrode system and linear rotating electrode system, and increases the number of jets by increasing the contact area between the solution and the spinneret in one or two dimensions to increase the productivity ; The above disclosed technologies can theoretically realize the rapid production of electrospinning, but the actual application effect is not very good. The field is not optimistic; in the open design of the bubble electrospinning device and the first generation of "nano spider" series equipment, due to the high volatility of the spinning solution, it is impossible to effectively protect the solution in the liquid supply tank. As a result, the concentration of the solution and the diameter of the fiber in the process of electrospinning fibers change greatly with the time of electrospinning, resulting in differences in the performance of the same batch of products, and the electrodes used in the first generation of "nano spider" series equipment are immersed in the solution to be spun 100% utilization of the spinning solution cannot be realized. Although the second-generation "nano-spider" equipment produced by ELMARCO adopts a static linear electrode system design, which avoids the solvent volatilization of the spinning solution of the first-generation equipment, it still Failed to achieve effective improvement of spinning solution utilization and product performance

Method used

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Examples

Experimental program
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Effect test

Embodiment 1

[0011] The main structure of this embodiment includes a motor 1, a liquid brush 2, an insulating tape 3, a metal shaft 4, a metal ring electrode 5, micro-nano fibers 6, a metal collector 7, a high-voltage power supply negative pole 8, an insulating pulley 9, and a high-voltage power supply positive pole 10 , insulating shaft 11, high voltage power supply 12, liquid supply system 13, shunt pipe 14, collecting substrate 15, feeding drum 16 and discharging drum 17; round hanging metal shaft 4 is fixedly installed with 4-8 groups of concentric metal The ring electrode 5 and one end of the metal shaft 4 are electrically connected to the high voltage power supply 12 through the positive pole 10 of the high voltage power supply; 4-8 sets of concentric insulating pulleys 9 are fixedly installed on the insulating shaft 11, and the output shaft of the motor 1 is linked with the insulating shaft 11 and drives All the insulated pulleys 9 rotate, and the insulated pulleys 9 rotate through t...

Embodiment 2

[0013] The present embodiment takes the polyvinylpyrrolidone PVP solution as an example to describe in detail, setting the ambient temperature to be 24.5°C, and the relative humidity of the environment is 43%RH, and selecting the polyvinylpyrrolidone PVP solution with a mass percentage of 13% as the spinning solution; 13 grams of polyvinylpyrrolidone (PVP, its molecular weight is 1.3 million) particles are slowly added to 87 grams of absolute ethanol under magnetic stirring, magnetic stirring at room temperature for 4-5 hours and then standing for 0.5-1 hour to obtain a uniform The transparent mass percentage is the PVP electrospinning precursor solution of 13%; Then put the prepared PVP solution into the liquid supply system 13, turn on the motor 1 that controls the rotation of the insulating pulley 9, and make the insulating pulley 9 start to rotate and pass through the insulating pulley. Driven by the belt 3, the metal ring electrode 5 is rotated; then the high-voltage power...

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Abstract

The invention belongs to the technical field of electrostatic spinning equipment and relates to a compound annular electrode electrostatic spinning device. The main structure of the compound annular electrode electrostatic spinning device comprises a motor, a liquid brush, an insulating tape, a metal shaft, a metal annular electrode, micro-nano fibers, a metal collector, a high-voltage power supply negative electrode, an insulating pulley, a high-voltage power supply positive electrode, an insulating shaft, a high-voltage power supply, a liquid supply system, a distribution pipe, a connection substrate, a feeding rotary drum and a discharge rotary drum. The metal annular electrode is arranged on the metal shaft, and one end of the metal shaft is connected with the high-voltage power supply through the high-voltage power supply positive electrode; the insulating pulley is arranged on the insulating shaft, and the motor is in linkage with the insulating shaft, drives the insulating pulley to rotate and drives the metal annular electrode to rotate through the insulating tape; the distribution pipe is communicated with the liquid supply system, the liquid brush is arranged on an opening of the distribution pipe, the insulating tape penetrates through the liquid brush, the metal collector is located over the metal annular electrode, and the feeding rotary drum and the discharge rotary drum are arranged at two ends of the metal collector. The compound annular electrode electrostatic spinning device is simple in structure, reliable in principle, low in manufacturing cost, good in effect and environment-friendly, and conditions are easy to control.

Description

Technical field: [0001] The invention belongs to the technical field of electrospinning equipment, and relates to a compound ring electrode electrostatic spinning device for large-scale preparation of micro-nano fibers, which adopts a compound ring electrode fixed-point liquid supply method to realize rapid and large-scale preparation of electrostatic spinning micro-nano fibers. Background technique: [0002] At present, one of the main means of preparing continuous one-dimensional micro-nano fibers is electrospinning technology, which has good development prospects in the fields of filter materials, sound-absorbing and sound-absorbing materials, special protective clothing, electronic sensors, and textile engineering. Micro-nano fibers prepared by electrospinning have many characteristics such as large specific surface area and high porosity that are not possessed by fibers prepared by traditional stretching methods and melt-blown methods. Low, unable to meet the needs of i...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01D5/00
Inventor 龙云泽刘术亮黄渊源孙彬张红娣张君诚
Owner QINGDAO UNIV
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