The present invention provides a kind of spherical gold
powder and preparation method thereof, relate to the technical field of
precious metal powder preparation, the preparation method uses
aqua regia to prepare
chloroauric acid solution, and uses concentrated
hydrochloric acid to adjust pH to 1.5-2, then adds
ammonia water to adjust pH to 7-9, stirs 20-60s, then adds concentrated
hydrochloric acid to adjust pH to 1.2-2 again, obtains
mixed solution B;Then, the first dispersant solution is poured into the aforementioned
mixed solution B, after stirring evenly, the
mixed solution A of the second dispersant and the
reducing agent is quickly added, after stirring reaction,
sedimentation, post-treatment, obtains spherical gold
powder. Wherein, spherical gold powder of different sizes with a particle size within the range of 0.3-4 μm can be prepared by adjusting pH twice, and adding two different dispersants in a specific order of addition can make the prepared spherical gold powder uniform in particle size, good in dispersibility, regular in shape and smooth in surface. The preparation method reacts rapidly, the process is short and stable, and it has been stably expanded to 500g, which can realize large-scale industrial production.