Production process for preparing nanometer coal powder by using puffing and mechanical crushing

A production process and mechanical pulverization technology, used in nanotechnology, petroleum industry, grain processing, etc., can solve the problems of high energy consumption, low pulverization efficiency, large coal powder particles, etc., to reduce energy consumption and be widely used. Effect

Inactive Publication Date: 2013-08-07
SUZHOU CHIEN SHIUNG INST OF TECH
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AI Technical Summary

Problems solved by technology

[0003] At present, the production of nano-coal powder is mainly through ball mill pulverization and mechanical pulverization. In mechanical pulverization, jet mill is usually used for pulverization. The pulverization efficiency is not high, the energy consumption of the pulverization process is very large, and the pulverized coal particles obtained are too large to meet the production requirements. need

Method used

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Embodiment

[0019] Select anthracite, make granules, sieve, take about 1 kg of coal particles between 5 and 16 mesh, and use a low-temperature and high-pressure extruder for puffing treatment. The puffing pressure can be set at 5-10kgf / cm2, and the temperature is frozen to -20°C , use a general ball mill to crush the particles to more than 32 mesh (particle size <0.5mm), then use nitrogen or carbon dioxide as the protective gas, enter the closed circuit (inert gas protection type) fluidized bed jet mill for crushing and collecting step by step, and the preliminary crushing is 200~300 mesh, soak with an appropriate amount of 0.1mol / L NaOH solution at room temperature, rinse and filter with water after 30 minutes, then neutralize with a sufficient amount of 0.1mol / L hydrochloric acid, rinse with water, dry, and finally soak in benzene solvent Filtrate and recover the solvent benzene; after multiple times of puffing and jet crushing, when the particle size is 0.005-0.02 (mm) (about 600-2000 m...

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Abstract

The present invention provides a production process for preparing nanometer coal powder by using puffing and mechanical crushing. The production process comprises: carrying out a low temperature puffing treatment on selected coal particles under gas protection, crushing through a ball mill, carrying out jet mill crushing while carrying out chemical treatments such as alkali washing, acid washing, water washing and solvent extraction on the coal particles, and finally adopting a high energy nanometer impact mill to prepare the required coal nanometer particles. Compared with the production process in the prior art, the production process of the present invention has the following characteristics that: puffing and mechanical crushing are combined during the nanometer coal powder production process while the coal particle chemical treatments are performed during crushing, such that the prepared coal particles are fine, energy consumption during the production process is reduced, and the prepared nanometer coal powder has wide uses, can be used for compounding a novel fuel base material, can be separately adopted as a fuel or a fuel additive, can be adopted to replace carbon black products, and can further be separately adopted as a chemical industry intermediate.

Description

technical field [0001] The invention relates to a production process of nano-coal powder, in particular to a production process for preparing nano-coal powder by puffing and mechanical crushing, and belongs to the field of chemical industry. Background technique [0002] Coal is a natural organic mineral rock. In my country, coal reserves account for about 90% of the total petrochemical energy reserves, while the total reserves of oil and natural gas only account for 10%. Therefore, the utilization of coal is particularly important. Nanopowder, because of its extremely small size, the electronic structure and crystal structure of the surface are different from conventional particles. Therefore, it has properties that conventional particles and macroscopic objects do not have, such as surface effect, small size effect and macroscopic quantum tunneling effect, and exhibits a series of novel electrical, magnetic, optical, chemical and mechanical properties. Nanopowders have bee...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10L9/00C10L5/00B82Y40/00B02C21/00
Inventor 杨成德
Owner SUZHOU CHIEN SHIUNG INST OF TECH
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