Tantalum-tungsten material and preparation method thereof
An ingot casting and pickling technology, applied in the field of metal materials, can solve the problems of large grain size, poor plate homogeneity, uneven grain size, etc.
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[0024] The embodiment of the invention discloses a preparation method of a tantalum tungsten material, which includes the following steps:
[0025] 1) Perform the first forging of the tantalum-tungsten ingot, and the first heat treatment of the tantalum-tungsten ingot after the first forging;
[0026] 2) Perform a second forging of the tantalum-tungsten ingot obtained in step 1), and perform a second heat treatment on the tantalum-tungsten material after the second forging;
[0027] 3) Roll the tantalum-tungsten ingot obtained in step 2), and subject the rolled tantalum-tungsten ingot to a third heat treatment to obtain a tantalum-tungsten material.
[0028] According to the present invention, in the process of preparing the tantalum-tungsten material, it is first necessary to provide a tantalum-tungsten ingot. The preparation of the tantalum-tungsten ingot can be obtained by electron beam melting. The invention has no particular limitation on the preparation of the tantalum-tungsten i...
Example Embodiment
[0040] Example 1
[0041] 1) Tantalum 2.5 tungsten ingot is obtained by electron beam melting. The diameter of tantalum 2.5 tungsten ingot is 153mm and the length is 250~260mm. The composition of tantalum 2.5 tungsten ingot is shown in Table 1. Table 1 is tantalum 2.5 tungsten ingot The element composition data table;
[0042] Table 1 Elemental composition data table of tantalum 2.5 tungsten ingot
[0043]
[0044] 2) Ultrasonic detection of the tantalum 2.5 tungsten ingot obtained in step 1), and then heat the tantalum 2.5 tungsten ingot to 400°C, hold for 150 minutes, and perform axial upsetting, with an upsetting ratio of 1.6; then perform radial drawing, Obtain a tantalum 2.5 tungsten rod with a diameter of 100mm and a length of 450mm;
[0045] 3) Obtain the tantalum 2.5 tungsten rod in step 2) and divide it into 2 sections in the length direction. Take one section and remove the forging defects on the end face;
[0046] 4) Pickling the tantalum 2.5 tungsten rod obtained in step 3...
Example Embodiment
[0056] Example 2
[0057] 1) The tantalum 2.5 tungsten ingot is obtained by electron beam melting. The diameter of the tantalum 2.5 tungsten ingot is 155mm and the length is 242mm. The composition of the tantalum 2.5 tungsten ingot is shown in Table 2. Table 2 shows the elements of the tantalum 2.5 tungsten ingot Ingredient data sheet;
[0058] Table 2 Elemental composition data table of tantalum 2.5 tungsten ingot
[0059]
[0060] 2) Ultrasonic detection of the tantalum 2.5 tungsten ingot obtained in step 1), and then heat the tantalum 2.5 tungsten ingot to 500°C, hold for 150 minutes, and perform axial upsetting, with an upsetting ratio of 2.0; then perform radial drawing, Obtain a tantalum 2.5 tungsten rod with a diameter of 100mm and a length of 443mm;
[0061] 3) Obtain the tantalum 2.5 tungsten rod in step 2) and divide it into 2 sections in the length direction. Take one section and remove the forging defects on the end face;
[0062] 4) Pickling the tantalum 2.5 tungsten rod ...
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