Formation processing method for improving low-voltage formed foil water resistance
A chemical formation treatment and foil formation technology, which is applied in the direction of metal surface removal regulations, electrical components, electrolytic capacitors, etc., can solve the problems of unstable product performance, poor water resistance, etc., and achieve the effect of prolonging storage time and capacitor life, and improving water resistance
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Embodiment 1
[0015] Example 1: Take the corroded aluminum foil with a purity of 99.9%, place the aluminum foil in a 0.5% adipate aqueous solution by mass percentage, dip it for 3 minutes at 40°C, and take out the adipate with a mass percentage of 3%. In aqueous solution of ammonium diacid and adipate, at 65°C, current density 20mA / cm 2 , Under the condition of a voltage of 48V, perform primary formation for 20 minutes, then take it out and wash it for the first time, then heat-treat the aluminum foil after the first washing at 400°C for 1 minute, and then place the aluminum foil after the high-temperature treatment in In a mixed aqueous solution of 1% ammonium adipate and 0.1% dihydrogen phosphate by mass, at 85°C and a current density of 20mA / cm 2 , Under the condition of a voltage of 48V, the secondary formation was carried out for 5 minutes, and the aluminum foil was taken out for the second washing, and the aluminum foil after the second washing was treated in a phosphoric acid solutio...
Embodiment 2
[0016] Example 2: Take the corroded aluminum foil with a purity of 99.9%, place the aluminum foil in a 2% adipate aqueous solution by mass percentage, dip it for 3 minutes at 60°C, take out the adipate with a mass percentage of 10% In the aqueous solution of ammonium diacid and adipate, at 85°C, current density 20mA / cm 2 , Under the condition of a voltage of 48V, carry out the first-stage chemical conversion for 20 minutes, then take it out for the first water washing, and then perform the high-temperature heat treatment at 550°C for 5 minutes on the aluminum foil after the first water washing, and then place the aluminum foil after the high-temperature treatment in In a mixed aqueous solution of 5% ammonium adipate and 1% dihydrogen phosphate by mass, at 85°C and a current density of 20mA / cm 2 , Under the condition of a voltage of 48V, the secondary formation was carried out for 5 minutes, and the aluminum foil was taken out for the second washing, and the aluminum foil after...
Embodiment 3
[0017] Example 3: Take the corroded aluminum foil with a purity of 99.9%, place the aluminum foil in a 1% adipate aqueous solution by mass percentage, dip it for 3 minutes at 50°C, and take out the adipate with a mass percentage of 7%. In the aqueous solution of ammonium diacid and adipate, at 72°C, current density 20mA / cm 2 , Under the condition of a voltage of 48V, perform primary formation for 20 minutes, then take it out and wash it for the first time, then heat-treat the aluminum foil after the first water washing at 480°C for 3 minutes, and then place the aluminum foil after the high-temperature treatment in In a mixed aqueous solution of 3% ammonium adipate and 0.5% dihydrogen phosphate by mass, at 85°C and a current density of 20mA / cm 2 , Under the condition of a voltage of 48V, the secondary formation was carried out for 5 minutes, and the aluminum foil was taken out for the second washing, and the aluminum foil after the second washing was treated in a phosphoric aci...
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