Metamaterial substrate and preparation method thereof
A technology of metamaterials and substrates, applied in the field of metamaterials, can solve problems such as not being able to be used at high temperatures, and achieve the effects of low dielectric constant, small thermal expansion coefficient, and low dielectric loss
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Embodiment 1
[0025] Based on P 2 o 5 , ZnO, NaF, B 2 o 3 The total number of moles, the P 2 o 5 25%, ZnO 45%, NaF 20%, B 2 o 3 Mix 10% ingredients, add ethanol for ball milling for 2 hours, dry, put into a corundum crucible, heat to 1400°C in a high-temperature electric furnace, and keep warm for two hours to clarify and homogenize the glass melt; pour the glass melt into water to quench After cooling, add ethanol and ball mill for 4 hours, dry and pass through a 200-mesh sieve to prepare glass powder; based on the total mass number of glass powder and silicon nitride powder, mix the glass powder with silicon nitride powder at 10wt% , add ethanol and wet mill for 8 hours, dry, pass through a 60-mesh sieve, and prepare a pre-sintered body; prepare the pre-sintered body into a flat material of the required shape and size by hot pressing and sintering, and the process parameters are: the highest sintering temperature is 1500 ℃, 30MPa, heat preservation for 1h; brush copper on one sur...
Embodiment 2
[0028] Based on P 2 o 5 , ZnO, NaF, B 2 o 3 The total number of moles, the P 2 o 5 35%, ZnO 35%, NaF 25%, B 3 o 3 Mix 5% ingredients, add ethanol for ball milling for 2 hours, dry, put into a corundum crucible, heat to 1400°C in a high-temperature electric furnace, and keep it warm for two hours to clarify and homogenize the glass melt; pour the glass melt into water to quench After cooling, add ethanol and ball mill for 4 hours, dry and pass through a 200-mesh sieve to prepare glass powder; based on the total mass number of glass powder and silicon nitride powder, mix the glass powder with silicon nitride powder at 15wt% , add ethanol and wet mill for 8 hours, dry, pass through a 60-mesh sieve, and prepare a pre-sintered body; prepare the pre-sintered body into a flat material of the required shape and size by hot pressing and sintering, and the process parameters are: the highest sintering temperature is 1500 ℃, 30MPa, heat preservation for 1h; brush copper on one s...
Embodiment 3
[0031] Based on P 2 o 5 , ZnO, NaF, B 2 o 3 The total number of moles, the P 2 o 5 30%, ZnO 40%, NaF 22%, B 2 o 3 Mix 8% ingredients, add ethanol for ball milling for 2 hours, dry, put into a corundum crucible, heat to 1400°C in a high-temperature electric furnace, and keep it warm for two hours to clarify and homogenize the glass melt; pour the glass melt into water to quench After cooling, add ethanol and ball mill for 4 hours, dry and pass through a 200-mesh sieve to prepare glass powder; based on the total mass number of glass powder and silicon nitride powder, mix the glass powder with silicon nitride powder at 15wt% , add ethanol and wet mill for 8 hours, dry, pass through a 60-mesh sieve, and prepare a pre-sintered body; prepare the pre-sintered body into a flat material of the required shape and size by hot pressing and sintering, and the process parameters are: the highest sintering temperature is 1500 ℃, 30MPa, heat preservation for 1h; brush copper on one s...
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