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Polybutylene succinate resin composition and its preparation method

A technology of polybutylene succinate and resin composition, which is applied in the field of polymer material modification, can solve the undiscovered problems of PBS impact resistance and tensile strength, and achieve the improvement of mechanical properties and heat resistance, High impact performance, good fluidity effect

Active Publication Date: 2013-11-06
BEIJING RISUN TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the current research, no relevant reports on the improvement of the impact resistance and tensile strength of PBS were found.

Method used

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  • Polybutylene succinate resin composition and its preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034]50wt% polybutylene succinate (melt index: 9g / 10min, test condition: 190°C, 2.16kg), 20wt% EPDM rubber (38% propylene content), 20wt% Malay Anhydride grafted polypropylene (maleic anhydride graft rate 3%), 1wt% aminosilane coupling agent (KH550) and 0.4wt% antioxidant β-(3,5-di-tert-butyl-4-hydroxy Phenyl)stearyl propionate (IRGANOX1076) and 0.6wt% tris(2,4-di-tert-butylphenyl)phosphite (IRGAFOS168) were stirred in a high-speed mixer for 5 minutes, and after mixing evenly, put After the twin-screw extruder, add 8wt% alkali-free glass fiber to the fiber inlet, and extrude to pelletize. The length-to-diameter ratio of the twin-screw extrusion equipment is 35, the controlled feeding speed is 8rpm, the screw speed is 200rpm, and the temperature of each partition of the screw barrel is 100°C for the first partition, 140°C for the second partition, 140°C for the third partition, and 140°C for the fourth partition. Zone 145°C, fifth zone 145°C, sixth zone 145°C, seventh zone 14...

Embodiment 2

[0036] 58.3wt% polybutylene succinate resin (melt index is 9g / 10min, test condition is 190°C, 2.16kg), 18wt% EPDM rubber (propylene content 32%), 5wt% Maleic anhydride grafted EPDM (maleic anhydride graft rate 2%), 0.5wt% epoxy silane coupling agent (KH570) and 0.2wt% antioxidant tris(2,4-di-tert-butyl phenyl) ester (IRGAFOS168) was stirred in a high-speed mixer for 4 minutes, after mixing evenly, after being put into a twin-screw extruder, 18wt% alkali-free glass fiber was added to the fiber inlet, and extruded to granulate. The aspect ratio of the twin-screw extrusion equipment is 32, the feeding speed is controlled at 8rpm, the screw speed is 300rpm, and the temperature of each zone of the screw barrel is 100°C for the first zone, 140°C for the second zone, 140°C for the third zone, and 140°C for the fourth zone. Zone 145°C, fifth zone 145°C, sixth zone 145°C, seventh zone 140°C, eighth zone 140°C, ninth zone 130°C, die head temperature 130°C, strands were watered and pelle...

Embodiment 3

[0038] 54wt% polybutylene succinate resin (melt index is 9g / 10min, test condition is 190 ℃, 2.16kg), 20wt% SBS, 10wt% maleic anhydride grafted SBS (maleic anhydride grafted Branch rate 3.2%), 0.5wt% epoxy silane coupling agent (KH570) and 0.5wt% antioxidant β-(3,5-di-tert-butyl-4-hydroxyphenyl) octadecanoic acid Alcohol ester (IRGANOX1076) was stirred in a high-speed mixer for 3 minutes. After mixing evenly, it was put into a twin-screw extruder, and 15wt% alkali-free glass fiber was added to the fiber inlet, and extruded to granulate. The length-to-diameter ratio of the twin-screw extrusion equipment is 40, the feeding speed is controlled at 8rpm, the screw speed is 280rpm, and the temperature of each partition of the screw barrel is 100°C for the first partition, 140°C for the second partition, 140°C for the third partition, and 140°C for the fourth partition. Zone 145°C, fifth zone 145°C, sixth zone 145°C, seventh zone 140°C, eighth zone 140°C, ninth zone 130°C, die head te...

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Abstract

The invention discloses a high strength and toughening polybutylene succinate resin composition and its preparation method, as well as a product containing the polybutylene succinate resin composition. Due to adding of an elastomer, glassfiber and other components into polybutylene succinate, high impact performance can be obtained, and at the same time, the mechanical properties and thermal resistance of the obtained resin composition product can be improved. The obtained polybutylene succinate resin composition has the prominent advantages of good mechanical properties, good fluidity, good heat resistance, easy processing molding, biodegradability and the like, and is suitable for the field of mobile phone shells, laptop shells and other electronic products. The preparation method of the polybutylene succinate resin composition has the characteristics of simple and continuous process and high production efficiency, and the prepared product has stable quality.

Description

technical field [0001] The present invention relates to the field of modification of polymer materials, in particular to a polybutylene succinate resin composition and a preparation method thereof and products comprising the polybutylene succinate resin composition, especially a polybutylene succinate resin composition A high-strength and toughened polybutylene succinate resin composition, a preparation method thereof, and products comprising the polybutylene succinate resin composition. Background technique [0002] Polybutylene succinate (PBS) is a new type of material with good mechanical properties, degradation properties and processing properties. It has a wide range of applications in the fields of material packaging, agriculture and biomedical polymers. prospect. However, pure PBS has highly hydrophobic and flexible molecular chains, and its shortcomings of high crystallinity, poor toughness and low strength limit its application in many fields. Therefore, in order ...

Claims

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Application Information

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IPC IPC(8): C08L67/02C08L53/02C08L23/16C08L75/04C08L77/00C08K7/14B29C47/92B29C48/92
CPCB29C48/022
Inventor 张英伟姜立忠石志哲冯清正潘小军
Owner BEIJING RISUN TECH CO LTD
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