Modified silanized metal surface pretreatment agent containing polyoxyethylene sorbitan monooleate and preparation method thereof

A technology of sorbitan and monooleate, which is applied in epoxy resin coatings, coatings, anti-corrosion coatings, etc., and can solve the problems of lack of "self-repair" performance, poor self-repair performance, and weak corrosion resistance, etc. problem, to achieve the effect of no hanging dust, strong adhesion and strong corrosion resistance

Inactive Publication Date: 2013-12-18
ANHUI PROVINCE SUZHOU CITY LONGHUA MACHINERY MFG
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The silane treatment of metal surfaces has broad application prospects, but the silane film formed by the existing technology has defects ...

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Weigh raw materials (kg) according to the following weight: 100 deionized water, 12 modified coupling agents, 14 propylene glycol, 25 silane coupling agents KH-151, 35 silane coupling agents KH-42, 1.5 dicumyl peroxide , sodium perfluorooctanoate 0.0024, tree ash 0.4, water-based epoxy resin emulsion 5, sodium carboxymethylcellulose 2, polyoxyethylene sorbitan monooleate 0.6, phenylethyl biphenol polyoxyethylene ether 0.4, lanthanum acetate 0.007 , Phytic acid 0.25,

[0023] Preparation:

[0024] (1) Preparation of modified coupling agent

[0025] Add water-soluble nano-scale silica sol to 4-5% nano-zinc powder, 3-5% iron oxide, 4-6% 2-aminoethylheptadecenyl imidazoline, mix and heat to 95-115°C, 20-30 After a few minutes, it can be cooled;

[0026] (2) Add the silane coupling agent KH-151 first according to the proportion of the formula in the stirring tank, then add dicumyl peroxide, stir at 300-400rpm for 3-4 minutes, then add the silane coupling agent KH -42,...

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PUM

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Abstract

The invention discloses a modified silanized metal surface pretreatment agent containing polyoxyethylene sorbitan monooleate. The pretreatment agent is prepared from the following raw materials in parts by weight: 100 parts of deionized water, 10-15 parts of modified coupling agent, 10-15 parts of propylene glycol, 30-40 parts of silane coupling agent KH-42, 20-30 parts of silane coupling agent KH-151, 1-2 parts of dicumyl peroxide, 0.002-0.003 part of perfluorooctyl sodium sulfonate, 0.3-0.5 part of wood ash, 4-6 parts of water-borne epoxy resin emulsion, 2-3 parts of sodium carboxymethyl cellulose, 0.4-1.0 part of polyoxyethylene sorbitan monooleate, 0.2-0.6 part of phenylethyl diphenol polyoxyethylene ether, 0.005-0.01 part of lanthanum acetate and 0.1-0.3 part of phytic acid. A final product is obtained by modifying the coupling agent, compounding, adding auxiliaries and carrying out distribution, mixing and reaction. The modified silanized surface pretreatment agent has the characteristics of no toxicity, environment friendliness, convenience in use, compact and uniform silane film, strong adhesion and good corrosion resistance.

Description

technical field [0001] The invention relates to metal surface treatment agent technology, in particular to a modified silylated metal surface pretreatment agent containing polyoxyethylene sorbitan monooleate and a preparation method thereof. Background technique [0002] Corrosion of metal materials occurs around us every moment. According to statistics, about 10% of metal materials are corroded and cannot be recycled every year. This not only causes a huge waste of metal resources, but also poses a serious threat to normal production and personal safety. Surface treatment of metal materials is a commonly used anti-corrosion method. Method, the main method currently used for metal coating pretreatment is phosphating method. However, the traditional metal surface treatment methods have problems such as pollution to the environment due to the presence of toxic and harmful substances, and are no longer suitable for the increasingly high environmental requirements of human ...

Claims

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Application Information

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IPC IPC(8): C09D183/04C09D163/00C09D7/12C09D5/08
Inventor 杨家坤张德华徐勇
Owner ANHUI PROVINCE SUZHOU CITY LONGHUA MACHINERY MFG
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